1-([1,2,4]噻唑o[4,3-a]吡啶-3-基)乙基氨基甲酸-(S)-叔丁酯合成路线 （共 3 条）
反应条件
Lawesson's reagent in ethylene glycol dimethyl ether
T=80°C; 2 h;
参考文献
Moulin, Aline; Martinez, Jean; Fehrentz, Jean-Alain
Tetrahedron Letters, 2006 , vol. 47, # 43 p. 7591 - 7594
反应条件
1: 94 percent / BOP; N-methylmorpholine / CH2Cl2 / 2 h
2: 70 percent / Lawesson's reagent / 1,2-dimethoxy-ethane / 2 h / 80 °C
View Scheme
参考文献
Moulin, Aline; Martinez, Jean; Fehrentz, Jean-Alain
Tetrahedron Letters, 2006 , vol. 47, # 43 p. 7591 - 7594
反应条件
1: 94 percent / BOP; N-methylmorpholine / CH2Cl2 / 2 h
2: 70 percent / Lawesson's reagent / 1,2-dimethoxy-ethane / 2 h / 80 °C
View Scheme
参考文献
Moulin, Aline; Martinez, Jean; Fehrentz, Jean-Alain
Tetrahedron Letters, 2006 , vol. 47, # 43 p. 7591 - 7594
