N-(2-甲酰基-4-硝基苯基)乙酰胺合成路线 （共 11 条）
反应条件
1: concentrated hydrochloric acid 2: NaOH-solution View Scheme
参考文献
Cohn; Springer
Monatshefte fuer Chemie, 1903 , vol. 24, p. 91
反应条件
potassium hydroxide T=0°C;
参考文献
Journal of the Indian Chemical Society, , vol. 8, p. 59,65
参考文献
Journal of the Indian Chemical Society, , vol. 8, p. 59,65
反应条件
1: aqueous KOH-solution View Scheme
参考文献
Niyogy
Journal of the Indian Chemical Society, 1931 , vol. 8, p. 59,65
反应条件
1: 0.92 g / aq. HCl / 1.5 h / Heating
2: 0.18 g / 17.5 h / 150 - 160 °C
3: 1.14 g / POCl3 / 2.75 h / Heating
4: 0.57 g / H2 / Raney Ni / ethanol / 22 °C / 2663.3 Torr
5: 0.17 g / CH3COOK, H2 / 20percent Pd/C / ethanol / 24 °C / 2585.7 Torr
View Scheme
参考文献
Hutt, Marland P.; MacKellar, Forrest A.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, p. 349 - 352
反应条件
potassium hydroxide
T=0°C;
参考文献
Niyogy
Journal of the Indian Chemical Society, 1931 , vol. 8, p. 59,65
反应条件
1: 0.92 g / aq. HCl / 1.5 h / Heating
2: 0.18 g / 17.5 h / 150 - 160 °C
3: 94 percent / 1.) 1 N NaOH; 2.) 1 N HCl / 1.25 h / Heating
View Scheme
参考文献
Hutt, Marland P.; MacKellar, Forrest A.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, p. 349 - 352
反应条件
1: 0.92 g / aq. HCl / 1.5 h / Heating
2: 0.18 g / 17.5 h / 150 - 160 °C
3: 94 percent / 1.) 1 N NaOH; 2.) 1 N HCl / 1.25 h / Heating
4: 18.3 g / H2 / Raney Ni / dimethylformamide
View Scheme
参考文献
Hutt, Marland P.; MacKellar, Forrest A.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, p. 349 - 352
反应条件
1: 0.92 g / aq. HCl / 1.5 h / Heating
2: 0.18 g / 17.5 h / 150 - 160 °C
3: 1.14 g / POCl3 / 2.75 h / Heating
View Scheme
参考文献
Hutt, Marland P.; MacKellar, Forrest A.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, p. 349 - 352
反应条件
sulfuric acid
Deacetylation; 1 h; Heating;
参考文献
Dave, Rajesh H.; Hosangadi, Bhaskar D.
Tetrahedron, 1999 , vol. 55, # 37 p. 11295 - 11308
