2-(1H-吲哚-3-基)-N,N-二甲基乙酰胺合成路线 （共 15 条）
反应条件
1: 95 percent / concd. H2SO4 / 2 h / Heating 2: 80 percent / H2O / 40 h / 20 °C View Scheme
参考文献
Journal of Labelled Compounds and Radiopharmaceuticals, , vol. 39, # 8 p. 677 - 684
反应条件
1: 1)Ethyl chloroformate, Triethylamine / 1) from -12 to -15 deg C, 30 min., THF, 2) room temp., overnight, THF 2: 3.2 percent Chromat. / tetrakis(triphenylphosphine)nickel(0), triethylaluminum / tetrahydrofuran; toluene / 5 h / 80 °C View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 22, p. 1511 - 1518
反应条件
1: 92 percent Chromat. / benzene / 0.5 h / Ambient temperature 2: 1)Ethyl chloroformate, Triethylamine / 1) from -12 to -15 deg C, 30 min., THF, 2) room temp., overnight, THF 3: 3.2 percent Chromat. / tetrakis(triphenylphosphine)nickel(0), triethylaluminum / tetrahydrofuran; toluene / 5 h / 80 °C View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 22, p. 1511 - 1518
反应条件
Ni(PPh3)4; triethylaluminum in tetrahydrofuran; toluene T=80°C; 5 h; Product distribution;
参考文献
Journal of Heterocyclic Chemistry, , vol. 22, p. 1511 - 1518
反应条件
lithium aluminium tetrahydride in tetrahydrofuran; dichloromethane 48 h; Ambient temperature;
参考文献
Sintas, Jose A.; Vitale, Arturo A.
Journal of Labelled Compounds and Radiopharmaceuticals, 1997 , vol. 39, # 8 p. 677 - 684
