2,5-二氯-4,6-二甲基烟腈合成路线 （共 4 条）
反应条件
anhydrous tetramethylammonium chloride; trichlorophosphate in dichloromethane T=85°C; 5 h;
参考文献
BIAL - PORTELA and Cª., S.A.; RUSSO, Domenico; KISS, Laszlo Erno; WAHNON, Jorge Bruno Reis; LEARMONTH, David Alexander; ESZENYI, Tibor; ZIMMERMANN, Axel; SCHLUMMER, Bjoern; KREIS, Michael; REITER, Klaus
Patent: WO2013/89573 A1, 2013 ;
Location in patent: Page/Page column 15-16 ;
反应条件
1: 94 percent / sulfuryl chloride / CCl4 / 6 h / Heating 2: 76 percent / POCl3 / Heating View Scheme
参考文献
Chemistry of Heterocyclic Compounds, , vol. 40, # 3 p. 308 - 314
反应条件
1: morpholine / methanol / 65 °C 2: sulfuryl dichloride / acetonitrile / 0 - 20 °C 3: trichlorophosphate; anhydrous tetramethylammonium chloride / dichloromethane / 5 h / 85 °C View Scheme
反应条件
sulfuric acid Heating;
参考文献
Dyadyuchenko; Strelkov; Mikhailichenko; Zaplishny
Chemistry of Heterocyclic Compounds, 2004 , vol. 40, # 3 p. 308 - 314
