2,4,6-三甲氧基吡啶合成路线 （共 12 条）
反应条件
phosphorus pentachloride
参考文献
den Hertog et al.
Recueil des Travaux Chimiques des Pays-Bas, 1950 , vol. 69, p. 673,690
反应条件
sodium
T=140°C; 3.5 h; Heating;
参考文献
Kaneko, Chikara; Uchiyama, Keiji; Sato, Masayuki; Katagiri, Nobuya
Chemical & Pharmaceutical Bulletin, 1986 , vol. 34, # 9 p. 3658 - 3671
参考文献
ICI Australia Limited
Patent: US4631081 A1, 1986 ;
反应条件
lithium aluminium tetrahydride in diethyl ether
6 h; Heating;
参考文献
Chambers, Richard D.; Khalil, Ali; Murray, Christopher B.; Sandford, Graham; Batsanov, Andrei S.; Howard, Judith A.K.
Journal of Fluorine Chemistry, 2005 , vol. 126, # 7 p. 1002 - 1008
反应条件
1: 63 percent / CF3CO2H, 30percent aq. H2O2 / H2O / 3 h
2: 73 percent / POCl3 / 4 h / Heating
3: 81 percent / Na / 3.5 h / 140 °C / Heating
View Scheme
参考文献
Kaneko, Chikara; Uchiyama, Keiji; Sato, Masayuki; Katagiri, Nobuya
Chemical & Pharmaceutical Bulletin, 1986 , vol. 34, # 9 p. 3658 - 3671
反应条件
sodium
7 h; Heating;
参考文献
Kaneko, Chikara; Uchiyama, Keiji; Sato, Masayuki; Katagiri, Nobuya
Chemical & Pharmaceutical Bulletin, 1986 , vol. 34, # 9 p. 3658 - 3671
反应条件
1: 99 percent / NaOMe / 48 h / Heating
2: 25 percent / LiAlH4 / diethyl ether / 6 h / Heating
View Scheme
参考文献
Chambers, Richard D.; Khalil, Ali; Murray, Christopher B.; Sandford, Graham; Batsanov, Andrei S.; Howard, Judith A.K.
Journal of Fluorine Chemistry, 2005 , vol. 126, # 7 p. 1002 - 1008
反应条件
1: 73 percent / POCl3 / 4 h / Heating
2: 81 percent / Na / 3.5 h / 140 °C / Heating
View Scheme
参考文献
Kaneko, Chikara; Uchiyama, Keiji; Sato, Masayuki; Katagiri, Nobuya
Chemical & Pharmaceutical Bulletin, 1986 , vol. 34, # 9 p. 3658 - 3671
反应条件
1: concentrated aqueous hydrochloric acid / Durchleiten von Chlorwasserstoff und Behandeln der Reaktionsloesung mit Natriumnitrit
2: methanol
View Scheme
参考文献
den Hertog et al.
Recueil des Travaux Chimiques des Pays-Bas, 1950 , vol. 69, p. 673,690
参考文献
den Hertog et al.
Recueil des Travaux Chimiques des Pays-Bas, 1950 , vol. 69, p. 673,690
