2-甲氧基-6-(三氟甲基)烟酸合成路线 （共 2 条）
反应条件
in methanol
48 h; Heating / reflux;
参考文献
Blackaby, Wesley Peter; Castro Pineiro, Jose Luis; Lewis, Richard Thomas; Naylor, Elizabeth Mary; Street, Leslie Joseph
Patent: US2006/276655 A1, 2006 ;
Location in patent: Page/Page column 24 ;
US 20060276655 A1
反应条件
2,2,6,6-tetramethyl-piperidine; n-butyllithium; 1,2,2-trichloro-1,1,2-trichloro-ethane in tetrahydrofuran; hexanes
T=-78 - 20°C; 3.16667 h;
参考文献
Blackaby, Wesley Peter; Castro Pineiro, Jose Luis; Lewis, Richard Thomas; Naylor, Elizabeth Mary; Street, Leslie Joseph
Patent: US2006/276655 A1, 2006 ;
Location in patent: Page/Page column 24-25 ;
US 20060276655 A1
