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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
91633-30-6
合成路线
（共 21 条）
3319-15-1
4-甲氧基-α-甲基苯甲醇
→
反应条件
91633-30-6
反应条件
sodium azide; NbCl5 in acetonitrile T=20°C; 0.666667 h;
参考文献
Yadav; Bhunia, Dinesh C.; Vamshi Krishna; Srihari
Tetrahedron Letters, 2007 , vol. 48, # 47 p. 8306 - 8310
637-69-4
4-甲氧基苯乙烯
→
反应条件
91633-30-6
反应条件
sodium tetrahydroborate; sodium azide; ferric tartrate in tetrahydrofuran; water T=0°C; 0.583333 h; Inert atmosphere;
参考文献
Leggans, Erick K.; Barker, Timothy J.; Duncan, Katharine K.; Boger, Dale L.
Organic Letters, 2012 , vol. 14, # 6 p. 1428 - 1431
58287-11-9
→
反应条件
91633-30-6
反应条件
sodium azide in water T=60°C;
参考文献
Richard, John P.; Rothenberg, Marc E.; Jencks, William P.
Journal of the American Chemical Society, 1984 , vol. 106, # 5 p. 1361 - 1372
77525-91-8
→
反应条件
91633-30-6
反应条件
anhydrous iron chloride; trimethylsilylazide in dichloromethane T=20°C; 1 h; Inert atmosphere;
参考文献
Sawama, Yoshinari; Goto, Ryota; Nagata, Saori; Shishido, Yuko; Monguchi, Yasunari; Sajiki, Hironao
Chemistry - A European Journal, 2014 , vol. 20, # 9 p. 2631 - 2636
88563-46-6
→
反应条件
91633-30-6
+
108-95-2
苯酚
反应条件
Azide; acid in water T=20 - 24°C; different HN3/N3(1-) ratio; Product distribution;
参考文献
Richard, John P.; Rothenberg, Marc E.; Jencks, William P.
Journal of the American Chemical Society, 1984 , vol. 106, # 5 p. 1361 - 1372
32117-52-5
→
反应条件
91633-30-6
反应条件
sodium azide; tetrabutylammomium bromide; potassium carbonate in 1,4-dioxane T=110°C; 24 h;
参考文献
Barluenga, Jose; Tomas-Gamasa, Maria; Valdes, Carlos
Angewandte Chemie - International Edition, 2012 , vol. 51, # 24 p. 5950 - 5952
58287-11-9
→
反应条件
2906-29-8
+
91633-30-6
反应条件
sodium azide in water T=20 - 24°C; different azide concentrations; Product distribution;
参考文献
Richard, John P.; Rothenberg, Marc E.; Jencks, William P.
Journal of the American Chemical Society, 1984 , vol. 106, # 5 p. 1361 - 1372
88563-47-7
→
反应条件
15573-49-6
+
91633-30-6
反应条件
sodium azide in water T=20 - 24°C; different kinds of salts or none, also MeOH; Product distribution;
参考文献
Richard, John P.; Rothenberg, Marc E.; Jencks, William P.
Journal of the American Chemical Society, 1984 , vol. 106, # 5 p. 1361 - 1372
637-69-4
4-甲氧基苯乙烯
→
反应条件
91633-30-6
+
74447-44-2
反应条件
1: With N,N-dimethyl acetamide; (Ph3P)3RhCl; benzo[1,3,2]dioxaborole in dichloromethane T=0°C; 5 h; RefluxInert atmosphere; 2: With benzenesulphonyl azide; t-BuON=NOt-Bu in N,N-dimethyl-formamide T=80°C; Inert atmosphere; regioselective reaction;
参考文献
Kapat, Ajoy; Koenig, Andreas; Montermini, Florian; Renaud, Philippe
Journal of the American Chemical Society, 2011 , vol. 133, # 35 p. 13890 - 13893
88563-47-7
→
反应条件
3319-15-1
4-甲氧基-α-甲基苯甲醇
+
91633-30-6
反应条件
sodium azide; sodium acetate in water 20 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Amyes, Tina L.; Stevens, Ishmael W.; Richard, John P.
Journal of Organic Chemistry, 1993 , vol. 58, # 22 p. 6057 - 6066
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