1-甲基-2-苯基哌啶-4-酮合成路线 （共 5 条）
反应条件
molecular sieve; copper diacetate; anhydrous lithium acetate; palladium diacetate in N,N-dimethyl-formamide
T=100°C; 3 h;
参考文献
Revuelta, Julia; Cicchi, Stefano; Brandi, Alberto
Journal of Organic Chemistry, 2005 , vol. 70, # 14 p. 5636 - 5642
反应条件
T=400°C; P=0.2 Torr;
参考文献
Brandi, A.; Guarna, A.; Goti, A.; Sarlo, F. De
Tetrahedron Letters, 1986 , vol. 27, # 15 p. 1727 - 1730
反应条件
in water
12 h; Ambient temperature;
参考文献
Dyakov, M. Yu.; Sokolova, T. D.; Peretokin, A. V.; Moskovkin, A. S.; Unkovskii, B. V.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1991 , vol. 27, # 2 p. 183 - 186
Khimiya Geterotsiklicheskikh Soedinenii, 1991 , # 2 p. 224 - 227
反应条件
1: neat (no solvent) / 60 °C / In a sealed tube.
2: 46 percent / 400 °C / 0.2 Torr
View Scheme
参考文献
Brandi, A.; Guarna, A.; Goti, A.; Sarlo, F. De
Tetrahedron Letters, 1986 , vol. 27, # 15 p. 1727 - 1730
反应条件
1.) 60 deg C, 2d, 2.) 400 deg C, 0.15 Torr; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Brandi; Garro; Guarna; Goti; Cordero; De Sarlo
Journal of Organic Chemistry, 1988 , vol. 53, # 11 p. 2430 - 2434
