2-氯-3-甲基吡啶-N-氮氧化物合成路线 （共 7 条）
反应条件
triethylamine; trichlorophosphate in dichloromethane T=0 - 20°C; 4 h; Heating / reflux; Product distribution / selectivity;
参考文献
Bach, Peter; Marczynke, Michaela; Giordanetto, Fabrizio
European Journal of Organic Chemistry, 2012 , # 35 p. 6940 - 6952
反应条件
1: With triethylamine; trichlorophosphate in dichloromethane T=0 - 20°C; 5 h; Inert atmosphere; 2: With ammonium chloride; zinc in water T=120°C; Microwave irradiationSealed tubeInert atmosphere;
参考文献
Bach, Peter; Marczynke, Michaela; Giordanetto, Fabrizio
European Journal of Organic Chemistry, 2012 , # 35 p. 6940 - 6952
反应条件
triethylamine; trichlorophosphate in dichloromethane T=0 - 20°C; 4 h; Heating / reflux; Product distribution / selectivity;
参考文献
Bach, Peter; Marczynke, Michaela; Giordanetto, Fabrizio
European Journal of Organic Chemistry, 2012 , # 35 p. 6940 - 6952
反应条件
3-chloro-benzenecarboperoxoic acid in chloroform
T=0 - 20°C; 18 h; Inert atmosphere;
参考文献
Bach, Peter; Marczynke, Michaela; Giordanetto, Fabrizio
European Journal of Organic Chemistry, 2012 , # 35 p. 6940 - 6952
反应条件
1: concentrated sulfuric acid; aqueous hydrogen peroxide; sulfur trioxide
View Scheme
参考文献
Brown
Journal of the American Chemical Society, 1957 , vol. 79, p. 3565
反应条件
1: acetic acid / Erhitzen des Reaktionsprodukts mit wss. NaOH
2: concentrated sulfuric acid; aqueous hydrogen peroxide; sulfur trioxide
View Scheme
参考文献
Brown
Journal of the American Chemical Society, 1957 , vol. 79, p. 3565
参考文献
Brown
Journal of the American Chemical Society, 1957 , vol. 79, p. 3565
