in solid High Pressure; 2000 MPa at room temp.; extrd. (chloroform), chromy. (alumina); UV;
参考文献
Zhorin, V. A.; Nikiforov, G. A.; Khristyuk, A. L.; Enikolopyan, N. S.
Doklady Physical Chemistry (Translation of the physical chemistry section of Doklady Akademii Nauk), 1983 , vol. 271, p. 510 - 512
Doklady Akademii Nauk SSSR, 1983 , vol. 271, p. 650 - 652
in solid High Pressure; 2000 MPa at room temp.; extrd. (chloroform), chromy.(alumina); UV;
参考文献
Zhorin, V. A.; Nikiforov, G. A.; Khristyuk, A. L.; Enikolopyan, N. S.
Doklady Physical Chemistry (Translation of the physical chemistry section of Doklady Akademii Nauk), 1983 , vol. 271, p. 510 - 512
Doklady Akademii Nauk SSSR, 1983 , vol. 271, p. 650 - 652
in pyridine other Radiation; porphyrin, metal salt and pyridine were sealed in a glass tube, microwave power of 300 W, heated from room temp. to 180°C, stirred for 15min, cooled to 50°C; vessel was opened, decanted, TLC (silica gel), UV;
参考文献
Dean, Michelle L.; Schmink, Jason R.; Leadbeater, Nicholas E.; Brueckner, Christian
Dalton Transactions, 2008 , # 10 p. 1341 - 1345
in N,N-dimethyl-formamide react. of starting compd. in DMF according to A. D. Adler and F. R. Longo; J. Inorg. Nucl. Chem. 32, 2443 (1970); react. is monitored by thin-layer chromy., purifn. of Ni-complex by chromy. (Al2O3, CHCl3), slow recrystn. from CH2Cl2; characterized by UV and mass spectroscopy;
in methanol; chloroform tetraphenylporphyrin (300 mg) and Zn(OAc)2*2H2O (800 mg) refluxed (1 h) in CHCl3/MeOH (2:1); cooled; solvent removed (vac.); dissolved in CHCl3; chromd. (silica, CHCl3);
参考文献
Vail, Sean A.; Schuster, David I.; Guldi, Dirk M.; Isosomppi, Marja; Tkachenko, Nikolai; Lemmetyinen, Helge; Palkar, Amit; Echegoyen, Luis; Chen, Xihua; Zhang, John Z. H.
Journal of Physical Chemistry B, 2006 , vol. 110, # 29 p. 14155 - 14166
