反应条件
BuLi in diethyl ether; hexane inert atmosphere; addn. of BuLi (in hexane) to HN(i-Pr)2 (in ether), addn. of Sn-compd. (-78°C, during 5 min), warming to 25°C (over 2 h, stirring), addn. of MeLi in Et2O (-78°C); addn. to CH2Cl2 (-78°C), then addn. to water, washing of org. layer (aq. HCl, H2O), drying (MgSO4), solvent removal, chromy. (SiO2/hexane);
参考文献
Ashe, Arthur J. III; Klein, Wolfram; Rousseau, Roger
Organometallics, 1993 , vol. 12, p. 3225 - 3231
