反应条件
in diethyl ether Sn2Me6 (1.12 mmol) in Et2O treated with MeLi (1.20 mmol, 1.00 M soln. in Et2O) under Ar, stirred for 30 min at 0°C, TMTH (1.12 mmol) added via syringe, stirred for 30 min at room temp., cooled to 0°C, quenched with water; H2 collected with gas measuring device, GC analysis of org. layer;
参考文献
Reimann, Werner; Kuivila, Henry G.; Farah, Dan; Apoussidis, Theodorus
Organometallics, 1987 , vol. 6, p. 557 - 565
