反应条件
in tetrahydrofuran argon, added at -78°C, stirred at this temp. for 5 min, mixt was transfered to a soln. of water in THF, warmed to 25°C; solvent removed under vacuum, extracted with pentane, removal of the solvent, resulting oil was purified by glpc, elem. anal.;
参考文献
Ashe, Arthur J. III; Lohr, Lawrence L.; Al-Taweel, Samir M.
Organometallics, 1991 , vol. 10, p. 2424 - 2431
