6-氯-9-[2-脱氧-3,5-二-O-(4-甲基苯甲酰)-B-D-赤式-呋喃戊糖基]-9H-嘌呤合成路线 （共 15 条）
反应条件
N-benzyl-N,N,N-triethylammonium chloride; N,N-dimethyl-aniline; trichlorophosphate in acetonitrile T=80°C; 0.166667 h;
参考文献
Liu, Jiangqiong; Janeba, Zlatko; Robins, Morris J.
Organic Letters, 2004 , vol. 6, # 17 p. 2917 - 2919
参考文献
Brigham Young University
Patent: US4760137 A1, 1988 ;
反应条件
4 A molecular sieve; iodonium di(2,4,6-trimethylpyridine) perchlorate in acetonitrile 2 h;
参考文献
Journal of Organic Chemistry, , vol. 58, # 25 p. 7258 - 7262
反应条件
sodium hydride 1) acetonitrile, RT, 30 min; 2) acetonitrile, 18 h; Yield given. Multistep reaction;
参考文献
Hanna; Ramasamy; Robins; Revankar
Journal of Heterocyclic Chemistry, 1988 , vol. 25, # 6 p. 1899 - 1903
反应条件
1: (+/-)-10-camphorsulfonic acid 2: 38 percent / pyridine / Ambient temperature 3: 35 percent / 4 Angstroem molecular sieves / iodonium dicollidine perchlorate / acetonitrile / 2 h View Scheme
参考文献
Journal of Organic Chemistry, , vol. 58, # 25 p. 7258 - 7262
反应条件
1: 87 percent / pyridine / 2 h / 40 °C 2: 60 percent / POCl3; benzyltriethylammonium chloride; N,N-dimethylaniline / acetonitrile / 0.17 h / 80 °C View Scheme
参考文献
Organic Letters, , vol. 6, # 17 p. 2917 - 2919
反应条件
1: 87 percent / pyridine / 2 h / 40 °C 2: 60 percent / POCl3; benzyltriethylammonium chloride; N,N-dimethylaniline / acetonitrile / 0.17 h / 80 °C View Scheme
参考文献
Organic Letters, , vol. 6, # 17 p. 2917 - 2919
反应条件
potassium hydroxide; tri[2-(2-methoxyethoxy)ethyl]amine 1) MeCN, r.t.; Yield given. Multistep reaction;
参考文献
Carbohydrate Research, , vol. 216, p. 129 - 139
参考文献
Tetrahedron, , vol. 43, # 6 p. 1133 - 1140
反应条件
1.) acetonitrile, THF, 10 deg C, 40 min, 2.) acetonitrile, THF, 10 deg C, 10 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Heterocycles, , vol. 34, # 11 p. 2117 - 2121
