(1S,2R,5S)-(+)-薄荷基(R)-对甲苯亚磺酸盐合成路线 （共 11 条）
参考文献
Journal of Organic Chemistry, , vol. 32, p. 2059 - 2062
反应条件
trifluoroacetic acid in dichloromethane T=0 - 25°C; 1 h;
参考文献
European Journal of Organic Chemistry, , # 8 p. 1449 - 1458
反应条件
1: SOCl2 / 0 °C 2: 1) pyridine, 2) HCl / 1) Et2O, 0 deg C; 2) acetone View Scheme
参考文献
Journal of the American Chemical Society, , vol. 106, # 20 p. 6097 - 6098
反应条件
2-chloro-1-methyl-pyridinium iodide; triethylamine in dichloromethane 3 h; Heating;
参考文献
Furukawa, Mitsuru; Ohkawara, Tadashi; Noguchi, Yoshihide; Nishikawa, Masumi; Tomimatsu, Masahide
Chemical and Pharmaceutical Bulletin, 1980 , vol. 28, # 1 p. 134 - 141
反应条件
1: 92 percent / DEAD / tetrahydrofuran / 0.67 h / 0 - 25 °C 2: benzene / 1.5 h / 40 °C 3: tetrahydrofuran / 0.25 h / -70 °C 4: TFA / CH2Cl2 / 1 h / 0 - 25 °C View Scheme
参考文献
European Journal of Organic Chemistry, , # 8 p. 1449 - 1458
反应条件
1: benzene / 1.5 h / 40 °C 2: tetrahydrofuran / 0.25 h / -70 °C 3: TFA / CH2Cl2 / 1 h / 0 - 25 °C View Scheme
参考文献
European Journal of Organic Chemistry, , # 8 p. 1449 - 1458
反应条件
sulfuric acid in benzene 3 h; Heating;
参考文献
Furukawa, Mitsuru; Ohkawara, Tadashi; Noguchi, Yoshihide; Nishikawa, Masumi; Tomimatsu, Masahide
Chemical and Pharmaceutical Bulletin, 1980 , vol. 28, # 1 p. 134 - 141
反应条件
1: 65 percent / DEAD, Ph3P / benzene / 12 h / Ambient temperature 2: 23 percent / sulfuric acid / benzene / 3 h / Heating View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 28, # 1 p. 134 - 141
反应条件
1: 63 percent / triazol / acetonitrile / 18 h / Heating 2: 23 percent / sulfuric acid / benzene / 3 h / Heating View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 28, # 1 p. 134 - 141
反应条件
(i-Pr)2NMgBr 1.) ether, 2.) ether, -40 deg C; Multistep reaction;
参考文献
Chemistry Letters, , # 9 p. 1647 - 1650
