六氟-2,3-双(三氟甲基)-2,3-二醇合成路线 (共 9 条)
反应条件
potassium permanganate in water; acetone T=-30 - -20°C; 0.5 h;
参考文献
Knunyants, I. L.; Postovoi, S. A.; Delyagina, N. I.; Zeifman, Yu. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1987 , vol. 36, # 10 p. 2090 - 2095
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1987 , # 10 p. 2256 - 2261
反应条件
mercury T=100 - 120°C; Irradiation;
参考文献
Voss; Lichnock; Bargon
Journal of Fluorine Chemistry, 1997 , vol. 84, # 1 p. 35 - 40
反应条件
magnesium; mercury dichloride in N,N-dimethyl-formamide 1 h;
参考文献
Postovoi, S. A.; Vol'pin, I. M.; Mysov, E. I.; Zeifman, Yu. V.; German, L. S.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1989 , vol. 38, # 5.2 p. 1067 - 1070
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1988 , # 5 p. 1173 - 1176
反应条件
magnesium; mercury dichloride in tetrahydrofuran 1 h;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 36, # 10 p. 2225
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 10 p. 2396 - 2397
反应条件
aluminium; mercury dichloride
参考文献
Zefirov, Yu. V.; Vol'pin, I. M.; Postovoi, S. A.; German, L. S.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1987 , vol. 36, # 10 p. 2225
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1987 , # 10 p. 2396 - 2397
参考文献
Journal of Fluorine Chemistry, , vol. 23, p. 470
参考文献
Doklady Chemistry, , vol. 161, p. 393 - 395
Doklady Akademii Nauk SSSR, , vol. 161, # 6 p. 1356 - 1358
反应条件
magnesium; mercury in tetrahydrofuran T=18 - 20°C; 1 h;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 38, # 5.2 p. 1067 - 1070
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 5 p. 1173 - 1176
反应条件
pyridine T=24.9°C; var. solvents, temp., base; ΔH(excit), ΔS(excit); Thermodynamic dataMechanism;
参考文献
Canadian Journal of Chemistry, , vol. 61, p. 2264 - 2267