N-(2-氨基苯基)-n-(4-甲基苯基)胺盐酸盐合成路线 （共 12 条）
参考文献
Kommi, Damodara N.; Jadhavar, Pradeep S.; Kumar, Dinesh; Chakraborti, Asit K.
Green Chemistry, 2013 , vol. 15, # 3 p. 798 - 810
反应条件
sodium tetrahydroborate; palladium on activated charcoal in methanol; water
Ambient temperature;
参考文献
Cadogan, J. I. G.; Hutchison, H. Susan; McNab, Hamish
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 1407 - 1412
反应条件
hydrogen; triethylamine; palladium on activated charcoal in methanol
T=20°C; 0.5 h;
参考文献
Wrobel, Zbigniew; Kwast, Andrzej
Synlett, 2007 , # 10 p. 1525 - 1528
反应条件
1: t-BuOK / dimethylformamide / -60 °C
2: AcOH / dimethylformamide
3: 84 percent / Et3N; H2 / Pd/C / methanol / 0.5 h / 20 °C
View Scheme
参考文献
Wrobel, Zbigniew; Kwast, Andrzej
Synlett, 2007 , # 10 p. 1525 - 1528
反应条件
1: t-BuOK / dimethylformamide / -60 °C
2: AcOH / dimethylformamide
3: 84 percent / Et3N; H2 / Pd/C / methanol / 0.5 h / 20 °C
View Scheme
参考文献
Wrobel, Zbigniew; Kwast, Andrzej
Synlett, 2007 , # 10 p. 1525 - 1528
反应条件
1: 57 percent / Na / dimethylformamide; toluene / 2 h / 150 - 155 °C
2: 31 percent / sodium borohydride / Palladium-charcoal (5percent) / methanol; H2O / Ambient temperature
View Scheme
参考文献
Cadogan, J. I. G.; Hutchison, H. Susan; McNab, Hamish
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 1407 - 1412
反应条件
1: 57 percent / Na / dimethylformamide; toluene / 2 h / 150 - 155 °C
2: 31 percent / sodium borohydride / Palladium-charcoal (5percent) / methanol; H2O / Ambient temperature
View Scheme
参考文献
Cadogan, J. I. G.; Hutchison, H. Susan; McNab, Hamish
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 1407 - 1412
反应条件
T=750°C; P=0.001 Torr; 0.666667 h;
参考文献
Cadogan, J. I. G.; Hutchison, H. Susan; McNab, Hamish
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 1407 - 1412
反应条件
1: alcoholic ammonium sulfide / 120 °C / im Einschlussrohr
2: Destillation im Vakuum
View Scheme
参考文献
Heidensleben
Chemische Berichte, 1890 , vol. 23, p. 3454
反应条件
Destillation im Vakuum;
参考文献
Heidensleben
Chemische Berichte, 1890 , vol. 23, p. 3454
