(2-氰基-5-甲酰基苯基)硼酸合成路线 (共 3 条)
反应条件
tri-isopropoxy-borane; 2,2,6,6-tetramethylpiperidinyl-lithium
T=-60°C;
参考文献
Rozema, Michael J.; Fickes, Michael; McLaughlin, Maureen; Rohde, Bridget; McDermott, Todd
Tetrahedron Letters, 2006 , vol. 47, # 49 p. 8765 - 8768
反应条件
1: ethanol / Heating
2: 70 percent / LiTMP; B(OiPr)3 / -60 °C
View Scheme
参考文献
Rozema, Michael J.; Fickes, Michael; McLaughlin, Maureen; Rohde, Bridget; McDermott, Todd
Tetrahedron Letters, 2006 , vol. 47, # 49 p. 8765 - 8768
反应条件
palladium diacetate; potassium fluoride; 2-dicyclohexylphosphino-1,1'-biphenyl in methanol; toluene
T=68°C;
参考文献
Rozema, Michael J.; Fickes, Michael; McLaughlin, Maureen; Rohde, Bridget; McDermott, Todd
Tetrahedron Letters, 2006 , vol. 47, # 49 p. 8765 - 8768