5-苯基-1H-吡唑-4-胺双盐酸盐 H2O合成路线 （共 7 条）
反应条件
1: Heating
2: NH2NH2 / ethanol / 2 h / Heating
View Scheme
参考文献
Wilcoxen, Keith; Huang, Charles Q.; McCarthy, James R.; Grigoriadis, Dimitri E.; Chen, Chen
Bioorganic and Medicinal Chemistry Letters, 2003 , vol. 13, # 19 p. 3367 - 3370
反应条件
1: aq. HNO3
2: H2 / Pd-C / ethanol
View Scheme
参考文献
Kishimoto; Noguchi; Masuda
Chemical and Pharmaceutical Bulletin, 1976 , vol. 24, # 12 p. 3001 - 3010
反应条件
1: 1,2,3,4-tetrahydro-naphthalene
2: aq. HNO3
3: H2 / Pd-C / ethanol
View Scheme
参考文献
Kishimoto; Noguchi; Masuda
Chemical and Pharmaceutical Bulletin, 1976 , vol. 24, # 12 p. 3001 - 3010
反应条件
hydrazine in ethanol
Heating;
参考文献
Chen, Chen; Wilcoxen, Keith; McCarthy, James R.
Tetrahedron Letters, 1998 , vol. 39, # 45 p. 8229 - 8232
反应条件
hydrazine in ethanol
r.t., 1 h, reflux, 1 h; Yield given;
参考文献
Chen, Chen; Wilcoxen, Keith; McCarthy, James R.
Tetrahedron Letters, 1998 , vol. 39, # 45 p. 8229 - 8232
反应条件
1: dimethylformamide
2: Heating
3: NH2NH2 / ethanol / 2 h / Heating
View Scheme
参考文献
Wilcoxen, Keith; Huang, Charles Q.; McCarthy, James R.; Grigoriadis, Dimitri E.; Chen, Chen
Bioorganic and Medicinal Chemistry Letters, 2003 , vol. 13, # 19 p. 3367 - 3370
反应条件
1: dimethylformamide / r.t. to 40 deg C
2: Heating
3: NH2-NH2 / ethanol / r.t., 1 h, reflux, 1 h
View Scheme
参考文献
Chen, Chen; Wilcoxen, Keith; McCarthy, James R.
Tetrahedron Letters, 1998 , vol. 39, # 45 p. 8229 - 8232
