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乙二醇
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63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
91859-66-4
合成路线
（共 17 条）
91859-66-4
→
反应条件
3445-78-1
反应条件
1: Lawesson's reagent / toluene / 0.5 h / Heating 2: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 3: H2S / ethanol / pH 7.4 4: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 5: ethanol / Heating 6: I2; NaHCO3 / ethanol 7: Lawesson's reagent / toluene / 0.5 h / Heating 8: H2S / ethanol / pH 7.4 9: I2; NaHCO3 / ethanol 10: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 11: H2S / ethanol / pH 7.4 12: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 13: ethanol / Heating 14: I2; NaHCO3 / ethanol 15: Lawesson's reagent / toluene / 0.5 h / Heating 16: H2S / ethanol / pH 7.4 17: I2; NaHCO3 / ethanol 18: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 19: H2S / ethanol / pH 7.4 20: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 21: 77 percent / Lawesson's reagent / toluene / 3 h / Heating 22: ethanol / Heating 23: P4S10 / xylene / 2 h / Heating 24: ethanol / Heating 25: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 26: I2; NaHCO3 / ethanol 27: Lawesson's reagent / toluene / 0.5 h / Heating 28: H2S / ethanol / pH 7.4 29: P4S10 / xylene / 2 h / Heating 30: ethanol / Heating 31: P4S10 / xylene / 2 h / Heating 32: ethanol / Heating 33: P4S10 / xylene / 2 h / Heating 34: ethanol / Heating 35: I2; NaHCO3 / ethanol 36: H2S / ethanol / pH 7.4 37: P4S10 / xylene / 2 h / Heating 38: ethanol / Heating 39: P4S10 / xylene / 2 h / Heating View Scheme
参考文献
Pregnolato, Massimo; Terreni, Marco; Ubiali, Daniela; Pagani, Giuseppe; Borgna, Pietro; Pastoni, Fiorenzo; Zampollo, Fabrizio
Farmaco, 2000 , vol. 55, # 11-12 p. 669 - 679
100-39-0
溴化苄
+
4337-60-4
异噻唑并[5,4-b]吡啶-3-醇
→
反应条件
91859-66-4
反应条件
N-ethyl-N,N-diisopropylamine in methanol T=20°C;
参考文献
Furdas, Silviya D.; Shekfeh, Suhaib; Bissinger, Elisabeth-Maria; Wagner, Julia M.; Schlimme, Sonja; Valkov, Vassil; Hendzel, Michael; Jung, Manfred; Sippl, Wolfgang
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 12 p. 3678 - 3689
139356-49-3
→
反应条件
91859-66-4
反应条件
trichloro acetic anhydride in dichloromethane 0 to 25 deg C, 3.5 h;
参考文献
Wright; Abelman; Bostrom; Corbett
Tetrahedron Letters, 1992 , vol. 33, # 2 p. 153 - 156
154344-32-8
→
反应条件
91859-66-4
反应条件
mercury(II) diacetate; acetic acid in chloroform T=20°C; 0.5 h;
参考文献
Pregnolato, Massimo; Terreni, Marco; Ubiali, Daniela; Pagani, Giuseppe; Borgna, Pietro; Pastoni, Fiorenzo; Zampollo, Fabrizio
Farmaco, 2000 , vol. 55, # 11-12 p. 669 - 679
65282-42-0
→
反应条件
91859-66-4
反应条件
1: ethanol / Heating 2: I2; NaHCO3 / ethanol 3: Lawesson's reagent / toluene / 0.5 h / Heating 4: H2S / ethanol / pH 7.4 5: I2; NaHCO3 / ethanol 6: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 7: H2S / ethanol / pH 7.4 8: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 9: ethanol / Heating 10: I2; NaHCO3 / ethanol 11: Lawesson's reagent / toluene / 0.5 h / Heating 12: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 13: H2S / ethanol / pH 7.4 14: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 15: ethanol / Heating 16: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 17: ethanol / Heating 18: I2; NaHCO3 / ethanol 19: Lawesson's reagent / toluene / 0.5 h / Heating 20: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C View Scheme
参考文献
Pregnolato, Massimo; Terreni, Marco; Ubiali, Daniela; Pagani, Giuseppe; Borgna, Pietro; Pastoni, Fiorenzo; Zampollo, Fabrizio
Farmaco, 2000 , vol. 55, # 11-12 p. 669 - 679
154344-43-1
→
反应条件
91859-66-4
反应条件
1: Lawesson's reagent / toluene / 0.5 h / Heating 2: H2S / ethanol / pH 7.4 3: I2; NaHCO3 / ethanol 4: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 5: H2S / ethanol / pH 7.4 6: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 7: ethanol / Heating 8: I2; NaHCO3 / ethanol 9: Lawesson's reagent / toluene / 0.5 h / Heating 10: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 11: H2S / ethanol / pH 7.4 12: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 13: ethanol / Heating 14: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 15: ethanol / Heating 16: I2; NaHCO3 / ethanol 17: Lawesson's reagent / toluene / 0.5 h / Heating 18: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C View Scheme
参考文献
Pregnolato, Massimo; Terreni, Marco; Ubiali, Daniela; Pagani, Giuseppe; Borgna, Pietro; Pastoni, Fiorenzo; Zampollo, Fabrizio
Farmaco, 2000 , vol. 55, # 11-12 p. 669 - 679
154344-30-6
→
反应条件
91859-66-4
反应条件
1: H2S / ethanol / pH 7.4 2: I2; NaHCO3 / ethanol 3: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 4: H2S / ethanol / pH 7.4 5: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 6: ethanol / Heating 7: I2; NaHCO3 / ethanol 8: Lawesson's reagent / toluene / 0.5 h / Heating 9: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 10: H2S / ethanol / pH 7.4 11: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 12: ethanol / Heating 13: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 14: ethanol / Heating 15: I2; NaHCO3 / ethanol 16: Lawesson's reagent / toluene / 0.5 h / Heating 17: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C View Scheme
参考文献
Pregnolato, Massimo; Terreni, Marco; Ubiali, Daniela; Pagani, Giuseppe; Borgna, Pietro; Pastoni, Fiorenzo; Zampollo, Fabrizio
Farmaco, 2000 , vol. 55, # 11-12 p. 669 - 679
154344-45-3
→
反应条件
91859-66-4
反应条件
1: Lawesson's reagent / toluene / 0.5 h / Heating 2: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 3: H2S / ethanol / pH 7.4 4: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 5: ethanol / Heating 6: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 7: ethanol / Heating 8: I2; NaHCO3 / ethanol 9: Lawesson's reagent / toluene / 0.5 h / Heating 10: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C View Scheme
参考文献
Pregnolato, Massimo; Terreni, Marco; Ubiali, Daniela; Pagani, Giuseppe; Borgna, Pietro; Pastoni, Fiorenzo; Zampollo, Fabrizio
Farmaco, 2000 , vol. 55, # 11-12 p. 669 - 679
330667-57-7
→
反应条件
91859-66-4
反应条件
1: I2; NaHCO3 / ethanol 2: Lawesson's reagent / toluene / 0.5 h / Heating 3: H2S / ethanol / pH 7.4 4: I2; NaHCO3 / ethanol 5: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 6: H2S / ethanol / pH 7.4 7: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 8: ethanol / Heating 9: I2; NaHCO3 / ethanol 10: Lawesson's reagent / toluene / 0.5 h / Heating 11: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 12: H2S / ethanol / pH 7.4 13: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 14: ethanol / Heating 15: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 16: ethanol / Heating 17: I2; NaHCO3 / ethanol 18: Lawesson's reagent / toluene / 0.5 h / Heating 19: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C View Scheme
参考文献
Pregnolato, Massimo; Terreni, Marco; Ubiali, Daniela; Pagani, Giuseppe; Borgna, Pietro; Pastoni, Fiorenzo; Zampollo, Fabrizio
Farmaco, 2000 , vol. 55, # 11-12 p. 669 - 679
330667-58-8
→
反应条件
91859-66-4
反应条件
1: I2; NaHCO3 / ethanol 2: Lawesson's reagent / toluene / 0.5 h / Heating 3: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 4: H2S / ethanol / pH 7.4 5: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 6: ethanol / Heating 7: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 8: ethanol / Heating 9: I2; NaHCO3 / ethanol 10: Lawesson's reagent / toluene / 0.5 h / Heating 11: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C View Scheme
参考文献
Pregnolato, Massimo; Terreni, Marco; Ubiali, Daniela; Pagani, Giuseppe; Borgna, Pietro; Pastoni, Fiorenzo; Zampollo, Fabrizio
Farmaco, 2000 , vol. 55, # 11-12 p. 669 - 679
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