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63148-62-9
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
91859-66-4
合成路线
（共 17 条）
91859-79-9
→
反应条件
91859-66-4
反应条件
iodine; sodium hydrogencarbonate in ethanol
参考文献
Pregnolato, Massimo; Terreni, Marco; Ubiali, Daniela; Pagani, Giuseppe; Borgna, Pietro; Pastoni, Fiorenzo; Zampollo, Fabrizio
Farmaco, 2000 , vol. 55, # 11-12 p. 669 - 679
65282-55-5
→
反应条件
91859-66-4
反应条件
1: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 2: ethanol / Heating 3: I2; NaHCO3 / ethanol 4: Lawesson's reagent / toluene / 0.5 h / Heating 5: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C View Scheme
参考文献
Pregnolato, Massimo; Terreni, Marco; Ubiali, Daniela; Pagani, Giuseppe; Borgna, Pietro; Pastoni, Fiorenzo; Zampollo, Fabrizio
Farmaco, 2000 , vol. 55, # 11-12 p. 669 - 679
154344-24-8
→
反应条件
91859-66-4
反应条件
1: I2; NaHCO3 / ethanol 2: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 3: H2S / ethanol / pH 7.4 4: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 5: ethanol / Heating 6: I2; NaHCO3 / ethanol 7: Lawesson's reagent / toluene / 0.5 h / Heating 8: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 9: H2S / ethanol / pH 7.4 10: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 11: ethanol / Heating 12: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 13: ethanol / Heating 14: I2; NaHCO3 / ethanol 15: Lawesson's reagent / toluene / 0.5 h / Heating 16: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C View Scheme
参考文献
Pregnolato, Massimo; Terreni, Marco; Ubiali, Daniela; Pagani, Giuseppe; Borgna, Pietro; Pastoni, Fiorenzo; Zampollo, Fabrizio
Farmaco, 2000 , vol. 55, # 11-12 p. 669 - 679
154344-33-9
→
反应条件
91859-66-4
反应条件
1: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 2: H2S / ethanol / pH 7.4 3: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 4: ethanol / Heating 5: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 6: ethanol / Heating 7: I2; NaHCO3 / ethanol 8: Lawesson's reagent / toluene / 0.5 h / Heating 9: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C View Scheme
参考文献
Pregnolato, Massimo; Terreni, Marco; Ubiali, Daniela; Pagani, Giuseppe; Borgna, Pietro; Pastoni, Fiorenzo; Zampollo, Fabrizio
Farmaco, 2000 , vol. 55, # 11-12 p. 669 - 679
38521-46-9
2-巯基烟酸
→
反应条件
91859-66-4
反应条件
1.1: thionyl chloride / toluene / 3 h / Reflux 1.2: 20 °C 2.1: sulfuric acid / 100 °C 2.2: pH 11 / Reflux 2.3: pH 4 3.1: N-ethyl-N,N-diisopropylamine / methanol / 20 °C View Scheme
参考文献
Furdas, Silviya D.; Shekfeh, Suhaib; Bissinger, Elisabeth-Maria; Wagner, Julia M.; Schlimme, Sonja; Valkov, Vassil; Hendzel, Michael; Jung, Manfred; Sippl, Wolfgang
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 12 p. 3678 - 3689
50596-67-3
→
反应条件
91859-66-4
反应条件
1.1: sulfuric acid / 100 °C 1.2: pH 11 / Reflux 1.3: pH 4 2.1: N-ethyl-N,N-diisopropylamine / methanol / 20 °C View Scheme
参考文献
Furdas, Silviya D.; Shekfeh, Suhaib; Bissinger, Elisabeth-Maria; Wagner, Julia M.; Schlimme, Sonja; Valkov, Vassil; Hendzel, Michael; Jung, Manfred; Sippl, Wolfgang
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 12 p. 3678 - 3689
91859-66-4
→
反应条件
65282-42-0
反应条件
1: Lawesson's reagent / toluene / 0.5 h / Heating 2: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 3: H2S / ethanol / pH 7.4 4: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 5: ethanol / Heating 6: I2; NaHCO3 / ethanol 7: Lawesson's reagent / toluene / 0.5 h / Heating 8: H2S / ethanol / pH 7.4 9: I2; NaHCO3 / ethanol 10: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 11: H2S / ethanol / pH 7.4 12: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 13: ethanol / Heating 14: I2; NaHCO3 / ethanol 15: Lawesson's reagent / toluene / 0.5 h / Heating 16: H2S / ethanol / pH 7.4 17: I2; NaHCO3 / ethanol 18: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 19: H2S / ethanol / pH 7.4 20: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating View Scheme
参考文献
Pregnolato, Massimo; Terreni, Marco; Ubiali, Daniela; Pagani, Giuseppe; Borgna, Pietro; Pastoni, Fiorenzo; Zampollo, Fabrizio
Farmaco, 2000 , vol. 55, # 11-12 p. 669 - 679
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