1: bis(3,5-dimethyl-1-pyrazolyl)methane With n-butyllithium in tetrahydrofuran; Petroleum ether
T=-78°C; 2 h;
2: benzyl bromide in tetrahydrofuran
T=-78 - 20°C;
参考文献
Sanchez-Mendez, Alberto; Benito, Jose Maria; De Jesus, Ernesto; De La Mata, F. Javier; Flores, Juan C.; Gomez, Rafael; Gomez-Sal, Pilar
Dalton Transactions, 2006 , # 45 p. 5379 - 5389