1,9-二氮杂螺[5.5]十一烷-9-羧酸, 1-(2,2,2-三氟乙酰基)-, 1,1-二甲基乙酯合成路线 （共 3 条）
反应条件
water; potassium carbonate in methanol T=90°C; 2.5 h;
参考文献
Jenkins, Ian D.; Lacrampe, Fabienne; Ripper, Justin; Alcaraz, Lilian; Van Le, Phuc; Nikolakopoulos, George; De Leone, Priscila Almeida; White, Rodney H.; Quinn, Ronald J.
Journal of Organic Chemistry, 2009 , vol. 74, # 3 p. 1304 - 1313
反应条件
1: With pyridine
2: With Grubb's 2nd generation catalyst
3: With hydrogen; palladium on activated charcoal in methanol
P=3102.89 Torr;
参考文献
Gracias, Vijaya; Gasiecki, Alan F.; Moore, Joel D.; Akritopoulou-Zanze, Irini; Djuric, Stevan W.
Tetrahedron Letters, 2006 , vol. 47, # 50 p. 8977 - 8980
反应条件
palladium 10 on activated carbon; hydrogen in methanol
T=20°C;
参考文献
Jenkins, Ian D.; Lacrampe, Fabienne; Ripper, Justin; Alcaraz, Lilian; Van Le, Phuc; Nikolakopoulos, George; De Leone, Priscila Almeida; White, Rodney H.; Quinn, Ronald J.
Journal of Organic Chemistry, 2009 , vol. 74, # 3 p. 1304 - 1313
