N,N-dimethylformamide dineopentyl acetal in acetonitrile
Heating;
参考文献
Van Beek, Rick; Zoombelt, Arjan P.; Jenneskens, Leonardas W.; Van Walree, Cornelis A.; De Mello Donega, Celso; Veldman, Dirk; Janssen, Rene A. J.
Chemistry - A European Journal, 2006 , vol. 12, # 31 p. 8075 - 8083
1.1: 36 percent / N-bromosuccinimide / CHCl3; acetic acid / 96 h / 20 °C
2.1: diisopropylamine; n-butyllithium / tetrahydrofuran; hexane / 2 h / 50 °C
2.2: 3.39 g / tetrahydrofuran; hexane / 2 h / 50 °C
3.1: 89 percent / N,N-dimethylformamide dineopentyl acetal / acetonitrile / Heating
View Scheme
参考文献
Van Beek, Rick; Zoombelt, Arjan P.; Jenneskens, Leonardas W.; Van Walree, Cornelis A.; De Mello Donega, Celso; Veldman, Dirk; Janssen, Rene A. J.
Chemistry - A European Journal, 2006 , vol. 12, # 31 p. 8075 - 8083
1.1: diisopropylamine; n-butyllithium / tetrahydrofuran; hexane / 2 h / 50 °C
1.2: 3.39 g / tetrahydrofuran; hexane / 2 h / 50 °C
2.1: 89 percent / N,N-dimethylformamide dineopentyl acetal / acetonitrile / Heating
View Scheme
参考文献
Van Beek, Rick; Zoombelt, Arjan P.; Jenneskens, Leonardas W.; Van Walree, Cornelis A.; De Mello Donega, Celso; Veldman, Dirk; Janssen, Rene A. J.
Chemistry - A European Journal, 2006 , vol. 12, # 31 p. 8075 - 8083
