3-氨基丙基三乙氧基硅烷合成路线 （共 65 条）
反应条件
triethylamine in toluene
T=100 - 110°C; 10 h;
参考文献
Bushuk, Boris A.; Bushuk, Sergei B.; Cherepennikova, Nadezhda F.; Douglas, William E.; Fukin, Georgii K.; Grigoriev, Iliya S.; Klapshina, Larisa G.; Van Der Lee, Arie; Semenov, Vladimir V.
Mendeleev Communications, 2004 , vol. 14, # 3 p. 109 - 111
反应条件
triethylamine in toluene
Heating;
参考文献
Bushuk, Boris A.; Bushuk, Sergei B.; Cherepennikova, Nadezhda F.; Douglas, William E.; Fukin, Georgii K.; Grigoriev, Iliya S.; Klapshina, Larisa G.; Van Der Lee, Arie; Semenov, Vladimir V.
Mendeleev Communications, 2004 , vol. 14, # 3 p. 109 - 111
反应条件
1: gamma-aminopropyltriethoxysilane With hypophosphorous acid in acetonitrile
2 h; Heating;
2: acetylene With nickel dichloride in acetonitrile
T=20°C; 2 h;
参考文献
Ribiere, Patrice; Bravo-Altamirano, Karla; Antczak, Monika I.; Hawkins, Jennifer D.; Montchamp, Jean-Luc
Journal of Organic Chemistry, 2005 , vol. 70, # 10 p. 4064 - 4072
反应条件
triethylamine in benzene
Heating;
参考文献
Voronkov, M. G.; Shirchin, B.; Monkhoobor, D.; Byamba, B.; Tuyaa, M.; et al.
J. Gen. Chem. USSR (Engl. Transl.), 1990 , vol. 60, # 5 p. 1099 - 1102,975 - 977
反应条件
in toluene
T=20°C; Inert atmosphereMolecular sieve 5Å;
参考文献
The Goodyear Tire and Rubber Company
Patent: EP2189464 A1, 2010 ;
Location in patent: Page/Page column 8 ;
反应条件
triethylamine in dichloromethane
24 h;
参考文献
Calero, Pilar; Aznar, Elena; Lloris, J. Manuel; Marcos, Maria D.; Martinez-Manez, Ramon; Ros-Lis, Jose V.; Soto, Juan; Sancenon, Felix
Chemical Communications, 2008 , # 14 p. 1668 - 1670
反应条件
in ethanol
3 h; Inert atmosphereReflux;
参考文献
Titinchi, Salam J.J.; Abbo, Hanna S.
Catalysis Today, 2013 , vol. 204, p. 114 - 124
反应条件
triethylamine in toluene
参考文献
Baigozhin,A. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1975 , vol. 45, p. 2350,2310
反应条件
1: in tetrahydrofuran
T=0 - 5°C; Addition; 3 h;
2: With Carbamonitrile; triethylamine in tetrahydrofuran
T=40°C; Elimination; 3 h;
参考文献
Yamamoto, Tamotsu; Sugiyama, Susumu; Akimoto, Kenji; Hayashi, Kiyoshi
Organic Preparations and Procedures International, 1992 , vol. 24, # 3 p. 346 - 349
反应条件
1: tetrahydrofuran / 3 h / 0 - 5 °C
2: DCDA, Et3N / tetrahydrofuran / 3 h / 40 °C
View Scheme
参考文献
Yamamoto, Tamotsu; Terada, Atsushi; Muramatsu, Takashi; Ikeda, Katsuya
Organic Preparations and Procedures International, 1994 , vol. 26, # 5 p. 555 - 557
