反应条件
1: (E)-1-chloro-8-phenyl-1-octene-3,5,7-triyne With n-butyllithium in tetrahydrofuran; hexane
T=-78°C; 1 h;
2: chloro-trimethyl-silane in tetrahydrofuran; hexane
T=-78 - 20°C;
参考文献
Metay, Estelle; Hu, Qian; Negishi, Ei-Ichi
Organic Letters, 2006 , vol. 8, # 25 p. 5773 - 5776