反应条件
1: C14H21BrSi With tert.-butyl lithium in diethyl ether; pentane
T=-78°C;
2: 1,5-Diphenylpentan-3-one in diethyl ether; pentane
T=-78 - 0°C;
3: in diethyl ether; N,N-dimethyl-formamide; pentane
T=80°C; Peterson allenation; Further stages.;
参考文献
Tsubouchi, Akira; Kira, Takashiro; Takeda, Takeshi
Synlett, 2006 , # 16 p. 2577 - 2580