反应条件
1: (E)-1-bromo-1-trimethylsilyl-2-phenylethene With tert.-butyl lithium in diethyl ether; pentane
T=-78°C;
2: 2-benzyl-3-phenylpropionaldehyde in diethyl ether; pentane
T=-78 - 0°C;
3: in diethyl ether; N,N-dimethyl-formamide; pentane
T=50°C; Peterson allenation; Further stages.;
参考文献
Tsubouchi, Akira; Kira, Takashiro; Takeda, Takeshi
Synlett, 2006 , # 16 p. 2577 - 2580