反应条件
1.1: n-BuLi; TMSCl / pentane / 0.25 h / -78 °C
1.2: n-BuLi / pentane; tetrahydrofuran / 0.5 h / -78 °C
1.3: 54 percent / aq. HCl / 0.5 h / 22 °C
2.1: 83 percent / 1,2-dichloro-benzene / 0.08 h / 205 °C / microwave irradiation
View Scheme
参考文献
Nicolaou; Li, Ang; Edmonds, David J.
Angewandte Chemie - International Edition, 2006 , vol. 45, # 42 p. 7086 - 7090
