1: N-methylethylamine hydroiodide With sodium hydrogencarbonate in water
T=8 - 15°C;
2: chloroformic acid 4-nitrophenyl ester in dichloromethane; water
T=25 - 30°C; 3 h;
参考文献
SUN PHARMACEUTICAL INDUSTRIES LIMITED; Patel, Hetalkumar Virendrabhai
Patent: WO2003/101917 A2, 2003 ;
Location in patent: Page 11 ;