triphenylphosphine; palladium diacetate in 1,2-dichloro-ethane; pentane; benzene
T=50°C; 4 h;
参考文献
Capuzzi, Marinella; Gambacorta, Augusto; Gasperi, Tecla; Loreto, M. Antonietta; Tardella, P. Antonio
European Journal of Organic Chemistry, 2006 , # 22 p. 5076 - 5082
1.1: nBuLi / tetrahydrofuran; hexane / 0.5 h / -78 °C
1.2: 68 percent / tetrahydrofuran; hexane / 0.33 h / -78 °C
2.1: 95 percent / PPh3 / Pd(OAc)2 / benzene; 1,2-dichloro-ethane; pentane / 4 h / 50 °C
View Scheme
参考文献
Capuzzi, Marinella; Gambacorta, Augusto; Gasperi, Tecla; Loreto, M. Antonietta; Tardella, P. Antonio
European Journal of Organic Chemistry, 2006 , # 22 p. 5076 - 5082
