1: hydrogenchloride / methanol; dichloromethane / 1 h / 40 °C 2: sodium hydroxide; hydroxylamine-o-sulphonic acid / ethanol; water / 0.5 h / 60 °C 3: sodium periodate / dichloromethane; water / 12 h / 0 °C View Scheme
参考文献
Anderson, Erin D.; Boger, Dale L.
Journal of the American Chemical Society, 2011 , vol. 133, # 31 p. 12285 - 12292
1: hydrogenchloride / methanol; dichloromethane / 1 h / 40 °C 2: sodium hydroxide; hydroxylamine-o-sulphonic acid / ethanol; water / 0.5 h / 60 °C 3: sodium periodate / dichloromethane; water / 12 h / 0 °C 4: chloroform / 14 h / 20 - 60 °C View Scheme
参考文献
Anderson, Erin D.; Boger, Dale L.
Journal of the American Chemical Society, 2011 , vol. 133, # 31 p. 12285 - 12292
1: hydrogenchloride / methanol; dichloromethane / 1 h / 40 °C
2: sodium hydroxide; hydroxylamine-o-sulphonic acid / ethanol; water / 0.5 h / 60 °C
3: sodium periodate / dichloromethane; water / 12 h / 0 °C
4: 1,4-dioxane / 6 h / 22 °C
View Scheme
参考文献
Anderson, Erin D.; Boger, Dale L.
Journal of the American Chemical Society, 2011 , vol. 133, # 31 p. 12285 - 12292