acetyl chloride; sodium nitrite in dichloromethane; water
T=0 - 20°C;
参考文献
Oliveri, Christopher G.; Gianneschi, Nathan C.; Nguyen, SonBinh T.; Mirkin, Chad A.; Stern, Charlotte L.; Wawrzak, Zdzislaw; Pink, Maren
Journal of the American Chemical Society, 2006 , vol. 128, # 50 p. 16286 - 16296
Oliveri, Christopher G.; Gianneschi, Nathan C.; Nguyen, SonBinh T.; Mirkin, Chad A.; Stern, Charlotte L.; Wawrzak, Zdzislaw; Pink, Maren
Journal of the American Chemical Society, 2006 , vol. 128, # 50 p. 16286 - 16296
Oliveri, Christopher G.; Gianneschi, Nathan C.; Nguyen, SonBinh T.; Mirkin, Chad A.; Stern, Charlotte L.; Wawrzak, Zdzislaw; Pink, Maren
Journal of the American Chemical Society, 2006 , vol. 128, # 50 p. 16286 - 16296
1: 75 percent / Y(OTf)3 / acetonitrile / 0.5 h / 20 °C
2: 86 percent / tetrahydrofuran / 0.5 h
3: 97 percent / S8 / tetrahydrofuran / 4 h
4: 88 percent / NaNO2; AcCl / CH2Cl2; H2O / 0 - 20 °C
View Scheme
参考文献
Oliveri, Christopher G.; Gianneschi, Nathan C.; Nguyen, SonBinh T.; Mirkin, Chad A.; Stern, Charlotte L.; Wawrzak, Zdzislaw; Pink, Maren
Journal of the American Chemical Society, 2006 , vol. 128, # 50 p. 16286 - 16296
Oliveri, Christopher G.; Gianneschi, Nathan C.; Nguyen, SonBinh T.; Mirkin, Chad A.; Stern, Charlotte L.; Wawrzak, Zdzislaw; Pink, Maren
Journal of the American Chemical Society, 2006 , vol. 128, # 50 p. 16286 - 16296
