N,N-二乙基-M-氨基苯甲醚合成路线 (共 22 条)
反应条件
ammonium formate; palladium on activated charcoal in water T=20°C; 1.6 h;
参考文献
Nacario, Ruel; Kotakonda, Shailaja; Fouchard, David M. D.; Tillekeratne, L. M. Viranga; Hudson, Richard A.
Organic Letters, 2005 , vol. 7, # 3 p. 471 - 474
反应条件
bis (triortho-tolylphosphine)palladium(II) chloride in toluene T=105°C; 4 h;
参考文献
Guram, Anil S.; Buchwald, Stephen L.
Journal of the American Chemical Society, 1994 , vol. 116, # 17 p. 7901 - 7902
反应条件
potassium phosphate; copper(l) iodide; CVT-2537 in dimethyl sulfoxide T=90°C; 24 h; Inert atmosphere;
参考文献
Zhang, Yu; Yang, Xinye; Yao, Qizheng; Ma, Dawei
Organic Letters, 2012 , vol. 14, # 12 p. 3056 - 3059
反应条件
NHC-Pd(II)-Im; potassium tert-butylate in tetrahydrofuran T=50°C; 6 h; Inert atmosphere;
参考文献
Chen, Wen-Xin; Shao, Li-Xiong
Journal of Organic Chemistry, 2012 , vol. 77, # 20 p. 9236 - 9239,4
Title/Abstract Full Text Show Details
Chen, Wen-Xin; Shao, Li-Xiong
Journal of Organic Chemistry, 2012 , vol. 77, # 20 p. 9236 - 9239
反应条件
sodium hydride in tetrahydrofuran T=20°C; 24 h;
参考文献
Kamino, Shinichiro; Ichikawa, Hayato; Wada, Shun-ichi; Horio, Yuka; Usami, Yoshihide; Yamaguchi, Takako; Koda, Toshiki; Harada, Aki; Shimanuki, Kazusa; Arimoto, Masao; Doi, Mitsunobu; Fujita, Yoshikazu
Bioorganic and Medicinal Chemistry Letters, 2008 , vol. 18, # 15 p. 4380 - 4384
反应条件
potassium tert-butylate in toluene T=135°C; 36 h;
参考文献
Beller; Breindl; Riermeier; Tillack
Journal of Organic Chemistry, 2001 , vol. 66, # 4 p. 1403 - 1412
反应条件
potassium tert-butylate in toluene T=135°C; 36 h;
参考文献
Beller; Breindl; Riermeier; Tillack
Journal of Organic Chemistry, 2001 , vol. 66, # 4 p. 1403 - 1412
反应条件
potassium hydroxide in dimethyl sulfoxide T=20 - 50°C;
参考文献
Zhang, Lei; Peng, Chen; Zhao, Dan; Wang, Yue; Fu, Hai-Jian; Shen, Qi; Li, Jian-Xin
Chemical Communications, 2012 , vol. 48, # 47 p. 5928 - 5930
反应条件
sodium t-butanolate; PdNaY in toluene T=135°C; Dehydrobromination; amination; 20 h; Title compound not separated from byproducts;
参考文献
Journal of Organometallic Chemistry, , vol. 592, # 2 p. 225 - 234
反应条件
1: 3-methoxy-aniline With sodium hydride in tetrahydrofuran T=0°C; 0.5 h; 2: ethyl iodide in tetrahydrofuran T=20°C; 3 h;
参考文献
Journal of Organic Chemistry, , vol. 71, # 17 p. 6414 - 6419