反应条件
1: 1.) Cl2, glacial AcOH / 1.) CCl4, 30-35 deg C, 5 min, 2.) acetone, reflux, 15 min 2: 91 percent / PCl5 / chlorobenzene / 1 h / 60 - 80 °C 3: 92 percent / Cl2 / CHCl3; CCl4 / 72 h / 20 - 25 °C 4: 92 percent / 1.) H2O, 2.) aq. NaClO4 / dioxane / 1 h / Heating 5: 95 percent / 1.) PCl5, 2.) aq. NaClO4 / chlorobenzene / 0.5 h / Heating 6: 40 percent / aq. NaOH / methanol / 0.17 h / Heating View Scheme
参考文献
Russian Journal of General Chemistry, , vol. 63, # 1.1 p. 62 - 65
Zhurnal Obshchei Khimii, , vol. 63, # 1 p. 87 - 92
