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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
联苯单乙酮
合成路线
（共 436 条）
368-47-8
苯基三氟硅烷
+
99-91-2
对氯苯乙酮
→
反应条件
92-91-1
联苯单乙酮
反应条件
1: phenyl-trifluoro-silane With tetrabutyl ammonium fluoride; palladium diacetate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in tert-butyl alcohol T=20°C; Hiyama cross-coupling reaction; 0.0833333 h; Inert atmosphereSealed vial; 2: para-chloroacetophenone in tert-butyl alcohol T=60°C; Hiyama cross-coupling reaction; Inert atmosphereSealed vial;
参考文献
Molander, Gary A.; Iannazzo, Laura
Journal of Organic Chemistry, 2011 , vol. 76, # 21 p. 9182 - 9187
79048-33-2
+
108-86-1
溴代苯
→
反应条件
92-91-1
联苯单乙酮
反应条件
[Pd{C6H4(CH2N(CH2Ph)2)}(μ-Br)]2; potassium carbonate in N,N-dimethyl-formamide T=100°C; Stille coupling; 0.0833333 h; Microwave irradiation;
参考文献
Hajipour, Abdol R.; Karami, Kazem; Rafiee, Fatemeh
Applied Organometallic Chemistry, 2012 , vol. 26, # 1 p. 27 - 31
1354047-47-4
+
99-90-1
4-溴苯乙酮
→
反应条件
92-91-1
联苯单乙酮
反应条件
palladium diacetate in water; toluene T=80°C; Suzuki-Miyaura coupling; 18 h; Inert atmosphere;
参考文献
Ligation, Carbene; Tai, Chia-Cheng; Chang, Ya-Ting; Tsai, Jie-Hong; Jurca, Titel; Yap, Glenn P. A.; Ong, Tiow-Gan
Organometallics, 2012 , vol. 31, # 2 p. 637 - 643
99-93-4
+
98-80-6
→
反应条件
92-91-1
联苯单乙酮
反应条件
SPHOS; tris-(dibenzylideneacetone)dipalladium(0); nonafluoro-n-butanesulfonyl fluoride; caesium carbonate in acetonitrile T=60°C; Suzuki-Miyaura Coupling; 15 h; Inert atmosphere;
参考文献
Ikawa, Takashi; Saito, Kozumo; Akai, Shuji
Synlett, 2012 , vol. 23, # 15 p. 2241 - 2246
4426-21-5
+
99-91-2
对氯苯乙酮
→
反应条件
92-91-1
联苯单乙酮
反应条件
triphenyl phosphite; K3PO4*3H2O; Ipr.HCl; palladium diacetate in tert-butyl alcohol T=80°C; 6 h; Inert atmosphere;
参考文献
Chen, Xiaofeng; Ke, Haihua; Chen, Yao; Guan, Changwei; Zou, Gang
Journal of Organic Chemistry, 2012 , vol. 77, # 17 p. 7572 - 7578
4426-21-5
+
99-90-1
4-溴苯乙酮
→
反应条件
92-91-1
联苯单乙酮
反应条件
triphenyl phosphite; K3PO4*3H2O; Ipr.HCl; palladium diacetate in tert-butyl alcohol T=80°C; 6 h; Inert atmosphere;
参考文献
Chen, Xiaofeng; Ke, Haihua; Chen, Yao; Guan, Changwei; Zou, Gang
Journal of Organic Chemistry, 2012 , vol. 77, # 17 p. 7572 - 7578
971-66-4
+
13329-40-3
→
反应条件
92-91-1
联苯单乙酮
反应条件
palladium diacetate; caesium carbonate in N,N-dimethyl-formamide T=50°C; Suzuki-Miyaura Coupling; 8 h; Inert atmosphere;
参考文献
Yang, Minghua; Gu, Yongbing; Wang, Yan; Zhao, Xiyu; Yan, Guobing
Chinese Journal of Chemistry, 2012 , vol. 30, # 10 p. 2581 - 2586,6
623-12-1
+
98-80-6
→
反应条件
92-91-1
联苯单乙酮
反应条件
Cl6Pd2(2-)*2C13H19N2(1+); tetrabutylammomium bromide; potassium carbonate in N,N-dimethyl-formamide T=100°C; 10 h;
参考文献
Hajipour, Abdol Reza; Dehbane, Ifa Mahboobi; Rafiee, Fatemeh
Applied Organometallic Chemistry, 2012 , vol. 26, # 12 p. 743 - 747
42030-75-1
+
98-80-6
→
反应条件
92-91-1
联苯单乙酮
反应条件
potassium phosphate; 1,1'-bis(diphenylphosphanyl)ferrocenenickel(II) chloride in toluene T=110°C; Suzuki-Miyaura Coupling; 24 h; Schlenk technique;
参考文献
Li, Xiao-Jian; Zhang, Jin-Ling; Geng, Yu; Jin, Zhong
Journal of Organic Chemistry, 2013 , vol. 78, # 10 p. 5078 - 5084
75-05-8
→
反应条件
92-91-1
联苯单乙酮
反应条件
[2,2']bipyridinyl; palladium (II) trifluoroacetate; water; trifluoroacetic acid in tetrahydrofuran T=80°C; 36 h; Inert atmosphereSchlenk technique;
参考文献
Wang, Xingyong; Liu, Miaochang; Xu, Long; Wang, Qingzong; Chen, Jiuxi; Ding, Jinchang; Wu, Huayue
Journal of Organic Chemistry, 2013 , vol. 78, # 11 p. 5273 - 5281
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