您好，欢迎来到魔法化学网！
合作交流
|
服务时间(9:30-18:00)
百科
百科
▼
百科
资讯
搜索
结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
首页
化合物百科
价格行情
资讯
化工导航
实验室工具
搜索
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-硝基联苯
合成路线
（共 331 条）
→
反应条件
92-52-4
联苯
+
92-93-3
4-硝基联苯
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene T=110°C; Stille cross-coupling; 48 h; Inert atmosphere;
参考文献
Journal of Organometallic Chemistry, , vol. 695, # 1 p. 103 - 110
→
反应条件
92-93-3
4-硝基联苯
反应条件
tetrabutylammomium bromide; palladium diacetate in water T=100°C; Suzuki-Miyaura coupling; 5 h;
参考文献
Basu, Basudeb; Biswas, Kinkar; Kundu, Sekhar; Ghosh, Sujit
Green Chemistry, 2010 , vol. 12, # 10 p. 1734 - 1738
636-98-6
4-硝基碘苯
+
88284-48-4
2-(三甲基硅)苯基三氟甲烷磺酸盐
→
反应条件
92-93-3
4-硝基联苯
反应条件
1: o-(trimethylsilyl)phenyl trifluoromethanesulfonate With potassium fluoride; 18-crown-6 ether; tri-n-butyl-tin hydride; hydroquinone in tetrahydrofuran T=20°C; 2 h; Inert atmosphere; 2: para-nitro iodo-benzene With copper(l) iodide; bis(η3-allyl-μ-chloropalladium(II)); triphenylphosphine in N,N-dimethyl-formamide T=60°C; Stille coupling; 16 h; Inert atmosphere;
参考文献
Lakshmi, B. Vasantha; Wefelscheid, Ulrike K.; Kazmaier, Uli
Synlett, 2011 , # 3 art. no. G36110ST, p. 345 - 348
99-99-0
对硝基甲苯
+
98-80-6
苯硼酸
→
反应条件
92-93-3
4-硝基联苯
反应条件
potassium carbonate in N,N-dimethyl acetamide; water T=100°C; Suzuki-Miyaura coupling; 16 h;
参考文献
Sreedhar; Yada, Divya; Reddy, P. Surendra
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 14-15 p. 2823 - 2836
368-47-8
苯基三氟硅烷
+
100-00-5
对硝基氯苯
→
反应条件
92-93-3
4-硝基联苯
反应条件
1: phenyl-trifluoro-silane With tetrabutyl ammonium fluoride; palladium diacetate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in tert-butyl alcohol T=20°C; Hiyama cross-coupling reaction; 0.0833333 h; Inert atmosphereSealed vial; 2: 1-chloro-4-nitro-benzene in tert-butyl alcohol T=60°C; Hiyama cross-coupling reaction; Inert atmosphereSealed vial;
参考文献
Molander, Gary A.; Iannazzo, Laura
Journal of Organic Chemistry, 2011 , vol. 76, # 21 p. 9182 - 9187
1354047-47-4
+
586-78-7
1-溴-4-硝基苯
→
反应条件
92-93-3
4-硝基联苯
反应条件
palladium diacetate in water; toluene T=80°C; Suzuki-Miyaura coupling; 18 h; Inert atmosphere;
参考文献
Ligation, Carbene; Tai, Chia-Cheng; Chang, Ya-Ting; Tsai, Jie-Hong; Jurca, Titel; Yap, Glenn P. A.; Ong, Tiow-Gan
Organometallics, 2012 , vol. 31, # 2 p. 637 - 643
100-02-7
对硝基苯酚
+
98-80-6
苯硼酸
→
反应条件
92-93-3
4-硝基联苯
反应条件
SPHOS; tris-(dibenzylideneacetone)dipalladium(0); nonafluoro-n-butanesulfonyl fluoride; caesium carbonate in acetonitrile T=60°C; Suzuki-Miyaura Coupling; 9 h; Inert atmosphere;
参考文献
Ikawa, Takashi; Saito, Kozumo; Akai, Shuji
Synlett, 2012 , vol. 23, # 15 p. 2241 - 2246
1232660-40-0
→
反应条件
92-93-3
4-硝基联苯
反应条件
N-hexadecyl-N,N,N-trimethylammonium bromide; palladium; triethylamine in water T=110°C; Suzuki-Miyaura Coupling; 0.5 h; Microwave irradiation; Reagent/catalyst;
参考文献
Civicos, Jose F.; Alonso, Diego A.; Najera, Carmen
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 14-15 p. 2771 - 2776
→
反应条件
92-93-3
4-硝基联苯
反应条件
tetrakis(triphenylphosphine) palladium(0); triethylamine; silver(l) oxide in methanol Suzuki-Miyaura cross-coupling reaction; 1.5 h; Heating;
参考文献
Cella, Rodrigo; Cunha, Rodrigo L. O. R.; Reis, Ana E. S.; Pimenta, Daniel C.; Klitzke, Clecio F.; Stefani, Helio A.
Journal of Organic Chemistry, 2006 , vol. 71, # 1 p. 244 - 250
591-50-4
碘苯
+
586-78-7
1-溴-4-硝基苯
→
反应条件
92-93-3
4-硝基联苯
反应条件
PEG 4000; palladium diacetate; potassium carbonate T=120°C; 12 h;
参考文献
Wang, Liang; Zhang, Yuhong; Liu, Leifang; Wang, Yanguang
Journal of Organic Chemistry, 2006 , vol. 71, # 3 p. 1284 - 1287
首页
上一页
1
...
9
10
11
12
13
14
15
...
34
下一页
末页
到第
页
确定
