4-(2-溴苯基)丁酰氯合成路线 （共 17 条）
反应条件
1: 95 percent / 170 °C
2: thionyl chloride / 0.75 h / Heating
View Scheme
参考文献
Adamczyk, Maciej; Watt, David S.; Netzel, Daniel A.
Journal of Organic Chemistry, 1984 , vol. 49, # 22 p. 4226 - 4237
反应条件
1: 85 percent / AlCl3 / CS2 / 3 h / Heating
2: 89 percent / NaBH4 / ethanol; tetrahydrofuran
3: 96 percent / p-toluenesulfonic acid / benzene / Heating
4: 98 percent / NiCl2<dppp>2 / diethyl ether / Heating
5: 99 percent / H2 / PtO2 / tetrahydrofuran / 1034.3 Torr
View Scheme
参考文献
Adamczyk, Maciej; Watt, David S.; Netzel, Daniel A.
Journal of Organic Chemistry, 1984 , vol. 49, # 22 p. 4226 - 4237
反应条件
1: CH2Cl2 / 0.25 h / 0 °C
2: 5 percent / K2CO3, tris(dibenzylideneacetone)dipalladium(0), tri-(o-tolyl)phosphine / toluene / 25 h / 110 °C
View Scheme
参考文献
Wolfe, John P.; Rennels, Roger A.; Buchwald, Stephen L.
Tetrahedron, 1996 , vol. 52, # 21 p. 7525 - 7546
反应条件
1: 85 percent / AlCl3 / CS2 / 3 h / Heating
2: 89 percent / NaBH4 / ethanol; tetrahydrofuran
3: 96 percent / p-toluenesulfonic acid / benzene / Heating
4: 98 percent / NiCl2<dppp>2 / diethyl ether / Heating
5: 97 percent / H2 / PtO2 / tetrahydrofuran / 1034.3 Torr
View Scheme
参考文献
Adamczyk, Maciej; Watt, David S.; Netzel, Daniel A.
Journal of Organic Chemistry, 1984 , vol. 49, # 22 p. 4226 - 4237
反应条件
1: 85 percent / AlCl3 / CS2 / 3 h / Heating
2: 89 percent / NaBH4 / ethanol; tetrahydrofuran
3: 96 percent / p-toluenesulfonic acid / benzene / Heating
View Scheme
参考文献
Adamczyk, Maciej; Watt, David S.; Netzel, Daniel A.
Journal of Organic Chemistry, 1984 , vol. 49, # 22 p. 4226 - 4237
反应条件
1: 85 percent / AlCl3 / CS2 / 3 h / Heating
2: 89 percent / NaBH4 / ethanol; tetrahydrofuran
View Scheme
参考文献
Adamczyk, Maciej; Watt, David S.; Netzel, Daniel A.
Journal of Organic Chemistry, 1984 , vol. 49, # 22 p. 4226 - 4237
反应条件
1: 85 percent / AlCl3 / CS2 / 3 h / Heating
2: 89 percent / NaBH4 / ethanol; tetrahydrofuran
3: 96 percent / p-toluenesulfonic acid / benzene / Heating
4: 97 percent / NiCl2<dppp>2 / diethyl ether / Heating
5: 98 percent / H2 / PtO2 / tetrahydrofuran / 1034.3 Torr
View Scheme
参考文献
Adamczyk, Maciej; Watt, David S.; Netzel, Daniel A.
Journal of Organic Chemistry, 1984 , vol. 49, # 22 p. 4226 - 4237
