反应条件
1: 2-Propenoic acid tert-butyl ester; cis-maleic acid With [{(η5-C5Me5)RhCl}2(μ-Cl)2]; silver carbonate in N,N-dimethyl-formamide
T=140°C; 1 h; Inert atmosphere;
2: methyl iodide With potassium carbonate in N,N-dimethyl-formamide
T=20°C; 3 h; Overall yield = 77 percent; Overall yield = 82 mg;
参考文献
Itoh, Masaki; Shimizu, Masaki; Hirano, Koji; Satoh, Tetsuya; Miura, Masahiro
Journal of Organic Chemistry, 2013 , vol. 78, # 22 p. 11427 - 11432