反应条件
1: 90 percent / potassium carbonate / 24 h / Heating
2: 74 percent / DIBAL-H / toluene / 3 h / -78 °C
3: 88 percent / sodium borohydride; trifluoroacetic acid / tetrahydrofuran / 1 h / 0 - 20 °C
4: 80 percent / 1,4-cyclohexadiene / Pd/C / ethanol; dioxane / 0.25 h / 20 °C
View Scheme
参考文献
Bulbule, Vivek J.; Koranne, Priti S.; Deshpande, Vishnu H.; Borate, Hanumant B.
Tetrahedron, 2007 , vol. 63, # 1 p. 166 - 170