1-(4-溴苯基)乙烷-1,2-二醇合成路线 （共 16 条）
反应条件
1: pyridine 2: NaOH / methanol / 2 h / 20 °C View Scheme
参考文献
Barlow, Thomas; Dipple, Anthony
Chemical Research in Toxicology, 1998 , vol. 11, # 1 p. 44 - 53
反应条件
Oxonereg;; 3,3'-diiodo-2,2',6,6'-tetramethoxy-4,4'-biphenyldicarboxylic acid in nitromethane T=30 - 35°C; 13 h;
参考文献
Seth, Saona; Jhulki, Samik; Moorthy, Jarugu Narasimha
European Journal of Organic Chemistry, 2013 , # 12 p. 2445 - 2452
反应条件
1: pyridine 2: NaOH / methanol / 2 h / 20 °C View Scheme
参考文献
Barlow, Thomas; Dipple, Anthony
Chemical Research in Toxicology, 1998 , vol. 11, # 1 p. 44 - 53
反应条件
1: With sodium periodate; acetic acid; lithium bromide
T=95°C; Prevost-Woodward reaction; 18 h;
2: With potassium carbonate in methanol
T=25°C; 24 h;
参考文献
Emmanuvel, Lourdusamy; Ali Shaikh, Tanveer Mahammad; Sudalai, Arumugam
Organic Letters, 2005 , vol. 7, # 22 p. 5071 - 5074
反应条件
sodium tetrahydroborate in ethanol
1 h;
参考文献
Mahajabeen, Pula; Chadha, Anju
Tetrahedron Asymmetry, 2011 , vol. 22, # 24 p. 2156 - 2160
反应条件
sodium tetrahydroborate in methanol
T=20°C;
参考文献
Kamal, Ahmed; Chouhan, Gagan
Tetrahedron Letters, 2004 , vol. 45, # 48 p. 8801 - 8805
反应条件
sulfuric acid; water in tetrahydrofuran
24 h;
参考文献
Pedragosa-Moreau; Morisseau; Zylber; Archelas; Baratti; Furstoss
Journal of Organic Chemistry, 1996 , vol. 61, # 21 p. 7402 - 7407
反应条件
1: With water in chloroform
T=40°C;
2: With water; sodium hydroxide in chloroform
T=40°C; 18 h;
参考文献
Jones, Kevin M.; Tomkinson, Nicholas C. O.
Journal of Organic Chemistry, 2012 , vol. 77, # 2 p. 921 - 928
反应条件
dihydrogen peroxide; lipase [PSLG6] in water
Heating;
参考文献
Sarma, Kuladip; Borthakur, Naleen; Goswami, Amrit
Tetrahedron Letters, 2007 , vol. 48, # 38 p. 6776 - 6778
反应条件
1: 95 percent / [bmim]Br / 0.5 h / 20 °C
2: 100 percent / NaBH4 / methanol / 20 °C
View Scheme
参考文献
Kamal, Ahmed; Chouhan, Gagan
Tetrahedron Letters, 2004 , vol. 45, # 48 p. 8801 - 8805
