N,N-二甲基-2-丁胺合成路线 (共 11 条)
反应条件
in anhydrous dichloroethane
T=20°C; 19 h; Heating / reflux;
参考文献
SANOFI-AVENTIS
Patent: US2008/146646 A1, 2008 ;
Location in patent: Page/Page column 9; 10 ;
反应条件
in anhydrous dichloroethane
T=20°C; 19 h; Heating / reflux;
参考文献
SANOFI-AVENTIS
Patent: US2008/146646 A1, 2008 ;
Location in patent: Page/Page column 9; 10 ;
反应条件
in anhydrous dichloroethane
T=20°C; 19 h; Heating / reflux;
参考文献
SANOFI-AVENTIS
Patent: US2008/146646 A1, 2008 ;
Location in patent: Page/Page column 9; 10 ;
反应条件
1: 2-cyclopropyl-5-nitro-1H-benzimidazole With sodium hydride in tetrahydrofuran
T=20°C; 3 h;
2: methyl iodide in tetrahydrofuran
T=20°C; 48 h;
参考文献
SANOFI-AVENTIS
Patent: US2008/146646 A1, 2008 ;
Location in patent: Page/Page column 12 ;
反应条件
ammonium formate; palladium 10 on activated carbon in ethanol
T=20°C; 72 h;
参考文献
SANOFI-AVENTIS
Patent: US2008/146646 A1, 2008 ;
Location in patent: Page/Page column 12 ;
反应条件
ammonium formate; palladium 10 on activated carbon in ethanol
T=20°C; 72 h;
参考文献
SANOFI-AVENTIS
Patent: US2008/146646 A1, 2008 ;
Location in patent: Page/Page column 12 ;
反应条件
1: 2-cyclopropyl-5-nitro-1H-benzimidazole With sodium hydride in tetrahydrofuran
T=20°C; 3 h;
2: methyl iodide in tetrahydrofuran
T=20°C; 48 h;
参考文献
SANOFI-AVENTIS
Patent: US2008/146646 A1, 2008 ;
Location in patent: Page/Page column 12 ;
反应条件
ammonium formate; palladium 10 on activated carbon in ethanol
T=20°C; 72 h;
参考文献
SANOFI-AVENTIS
Patent: US2008/146646 A1, 2008 ;
Location in patent: Page/Page column 12 ;
反应条件
ammonium formate; palladium 10 on activated carbon in ethanol
T=20°C; 72 h;
参考文献
SANOFI-AVENTIS
Patent: US2008/146646 A1, 2008 ;
Location in patent: Page/Page column 12 ;
反应条件
ammonium formate; palladium 10 on activated carbon in ethanol
T=20°C; 72 h;
参考文献
SANOFI-AVENTIS
Patent: US2008/146646 A1, 2008 ;
Location in patent: Page/Page column 12 ;