2-(氯甲基)-5-甲基-1,3-噻唑盐酸盐合成路线 （共 2 条）
反应条件
thionyl chloride in dichloromethane
T=0 - 35°C; 1 h;
参考文献
AURIGENE DISCOVERY TECHNOLOGIES LIMITED; TAKHI, Mohamed; HOSAHALLI, Subramanya; PANIGRAHI, Sunil Kumar; MAHADARI, Muni Kumar; KOTTAM, Chandrashekar Reddy; ABD RAHMAN, Noorsaadah; YUSOF, Rohana
Patent: WO2013/80222 A1, 2013 ;
Location in patent: Page/Page column 37 ;
反应条件
1: sodium tetrahydroborate / methanol / 1 h / 0 - 35 °C
2: thionyl chloride / dichloromethane / 1 h / 0 - 35 °C
View Scheme
参考文献
AURIGENE DISCOVERY TECHNOLOGIES LIMITED; TAKHI, Mohamed; HOSAHALLI, Subramanya; PANIGRAHI, Sunil Kumar; MAHADARI, Muni Kumar; KOTTAM, Chandrashekar Reddy; ABD RAHMAN, Noorsaadah; YUSOF, Rohana
Patent: WO2013/80222 A1, 2013 ;
