4'-乙基-4-联苯基羰基氯化物合成路线 （共 3 条）
反应条件
1.1: trimethyl borate / diethyl ether / 0.5 h / Heating
1.2: 30 percent / NaOH; PdCl2 / H2O; diethyl ether / 1 h / Heating
2.1: SOCl2 / 3 h / Heating
View Scheme
参考文献
Lucking; Tucci; Rudkevich; Rebek Jr.
Journal of the American Chemical Society, 2000 , vol. 122, # 37 p. 8880 - 8889
反应条件
1.1: trimethyl borate / diethyl ether / 0.5 h / Heating
1.2: 30 percent / NaOH; PdCl2 / H2O; diethyl ether / 1 h / Heating
2.1: SOCl2 / 3 h / Heating
View Scheme
参考文献
Lucking; Tucci; Rudkevich; Rebek Jr.
Journal of the American Chemical Society, 2000 , vol. 122, # 37 p. 8880 - 8889
反应条件
oxalyl dichloride; N,N-dimethyl-formamide in tetrahydrofuran; dichloromethane
1 h; Ambient temperature;
参考文献
Klein, Scott I.; Czekaj, Mark; Gardner, Charles J.; Guertin, Kevin R.; Cheney, Daniel L.; Spada, Alfred P.; Bolton, Scott A.; Brown, Karen; Colussi, Dennis; Heran, Christopher L.; Morgan, Suzanne R.; Leadley, Robert J.; Dunwiddie, Christopher T.; Perrone, Mark H.; Chu, Valeria
Journal of Medicinal Chemistry, 1998 , vol. 41, # 4 p. 437 - 450
