N-alpha-芴甲氧羰基-N-epsilon-叔丁氧羰基-D-赖氨酸合成路线 （共 6 条）
反应条件
sodium hydrogencarbonate in 1,4-dioxane 24 h;
参考文献
Watts, Paul; Wiles, Charlotte; Haswell, Stephen J; Pombo-Villar, Esteban
Tetrahedron, 2002 , vol. 58, # 27 p. 5427 - 5439
反应条件
in chloroform; acetonitrile
反应条件
1: 100 percent / CH2Cl2 / 0.58 h / 0 °C 2: 88 percent / Huenig's base; 1-hydroxybenzotriazole hydrate; 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride / CH2Cl2; dimethylformamide / 16 h / 18 °C 3: piperidine / tetrahydrofuran / 3 h / 18 °C View Scheme
参考文献
Banwell; McRae
Journal of Organic Chemistry, 2001 , vol. 66, # 20 p. 6768 - 6774
反应条件
trifluoroacetic acid in dichloromethane 0.5 h;
参考文献
Li, Yangmei; Dooley, Colette T.; Misler, Jaime A.; Debevec, Ginamarie; Giulianotti, Marc A.; Cazares, Margaret E.; Maida, Laura; Houghten, Richard A.
ACS Combinatorial Science, 2012 , vol. 14, # 12 p. 673 - 679
反应条件
1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride in dichloromethane T=20°C; 24 h;
参考文献
Watts, Paul; Wiles, Charlotte; Haswell, Stephen J; Pombo-Villar, Esteban
Tetrahedron, 2002 , vol. 58, # 27 p. 5427 - 5439
反应条件
1: trifluoroacetic acid / dichloromethane / 0.5 h 2: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.17 h / 20 °C View Scheme
参考文献
ACS Combinatorial Science, , vol. 14, # 12 p. 673 - 679
