5-氯-2-(4-甲氧基苯基)苯并[d]噻唑合成路线 (共 10 条)
反应条件
magnesium sulfate; copper(l) chloride in dimethyl sulfoxide
T=110°C; 6 h;
参考文献
Park, Namjin; Heo, Yumi; Kumar, Manian Rajesh; Kim, Yong; Song, Kwang Ho; Lee, Sunwoo
European Journal of Organic Chemistry, 2012 , # 10 p. 1984 - 1993
反应条件
in toluene
7 h; RefluxGreen chemistry;
参考文献
Sung, Gi Hyeon; Lee, In-Hye; Kim, Bo Ram; Shin, Dong-Soo; Kim, Jeum-Jong; Lee, Sang-Gyeong; Yoon, Yong-Jin
Tetrahedron, 2013 , vol. 69, # 17 p. 3530 - 3535
反应条件
ruthenium trichloride; 1-n-butyl-3-methylimidazolium hexafluorophosphate
T=80°C; 0.5 h;
参考文献
Fan, Xuesen; Wang, Yangyang; He, Yan; Zhang, Xinying; Wang, Jianji
Tetrahedron Letters, 2010 , vol. 51, # 27 p. 3493 - 3496
反应条件
samarium diiodide in tetrahydrofuran
T=20°C; 2 h;
参考文献
Zhong; Zhang; Chen
Journal of the Indian Chemical Society, 2001 , vol. 78, # 6 p. 316 - 318
反应条件
sodium hydroxide; potassium hexacyanoferrate(III) in ethanol; water
T=80 - 90°C;
参考文献
Bhuva, Hemal A.; Kini, Suvarna G.
Journal of Molecular Graphics and Modelling, 2010 , vol. 29, # 1 p. 32 - 37
反应条件
1: Lawesson's reagent / chlorobenzene / 3 h / Reflux
2: sodium hydroxide; potassium hexacyanoferrate(III) / ethanol; water / 80 - 90 °C
View Scheme
参考文献
Bhuva, Hemal A.; Kini, Suvarna G.
Journal of Molecular Graphics and Modelling, 2010 , vol. 29, # 1 p. 32 - 37
反应条件
1: pyridine / 2 h / Reflux
2: Lawesson's reagent / chlorobenzene / 3 h / Reflux
3: sodium hydroxide; potassium hexacyanoferrate(III) / ethanol; water / 80 - 90 °C
View Scheme
参考文献
Bhuva, Hemal A.; Kini, Suvarna G.
Journal of Molecular Graphics and Modelling, 2010 , vol. 29, # 1 p. 32 - 37
反应条件
1: pyridine / 2 h / Reflux
2: Lawesson's reagent / chlorobenzene / 3 h / Reflux
3: sodium hydroxide; potassium hexacyanoferrate(III) / ethanol; water / 80 - 90 °C
View Scheme
参考文献
Bhuva, Hemal A.; Kini, Suvarna G.
Journal of Molecular Graphics and Modelling, 2010 , vol. 29, # 1 p. 32 - 37
反应条件
1: aqueous sodium sulfide
2: NH4OAc / acetic acid / Heating
View Scheme
参考文献
Cossey,H.D. et al.
Journal of the Chemical Society, 1963 , p. 4322 - 4330
反应条件
in nitrobenzene
Heating;
参考文献
Cossey,H.D. et al.
Journal of the Chemical Society, 1963 , p. 4322 - 4330