7-甲氧基-3-硝基-2H-苯并吡喃合成路线 (共 4 条)
反应条件
sodium tetrahydroborate; silica gel in chloroform; isopropyl alcohol 0.25 h; Ambient temperature;
参考文献
Boye, Sophie; Pfeiffer, Bruno; Renard, Pierre; Rettori, Marie-Claire; Guillaumet, Gerald; Viaud, Marie-Claude
Bioorganic and Medicinal Chemistry, 1999 , vol. 7, # 2 p. 335 - 341
反应条件
1: 92 percent / NaBH4, SiO2 / CHCl3; propan-2-ol / 0.25 h / Ambient temperature 2: 90 percent / N2H4*H2O, Raney Ni / ethanol / 0.5 h / 45 °C View Scheme
参考文献
Boye, Sophie; Pfeiffer, Bruno; Renard, Pierre; Rettori, Marie-Claire; Guillaumet, Gerald; Viaud, Marie-Claude
Bioorganic and Medicinal Chemistry, 1999 , vol. 7, # 2 p. 335 - 341
反应条件
dibutylamine in chloroform
T=80°C; 24 h;
参考文献
Neirabeyeh, Mamdouh Al; Koussini, Rafik
Synthetic Communications, 1990 , vol. 20, # 6 p. 783 - 788
反应条件
di-n-butylamine hydrochloride in various solvent(s)
6.5 h; Heating;
参考文献
Dauzonne, Daniel; Royer, Rene
Synthesis, 1984 , # 4 p. 348 - 349