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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
922162-82-1
合成路线
（共 4 条）
922162-81-0
+
3282-30-2
三甲基乙酰氯
→
反应条件
922162-82-1
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane T=20°C; 16 h; Cooling with ice;
参考文献
Ichikawa, Masanori; Yokomizo, Aki; Itoh, Masao; Haginoya, Noriyasu; Sugita, Kazuyuki; Usui, Hiroyuki; Terayama, Koji; Kanda, Akira
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 17 p. 5207 - 5224
922162-80-9
→
反应条件
922162-82-1
反应条件
1: hydrogen / ethyl acetate / 7 h / 20 °C 2: 4-(N,N-dimethlyamino)pyridine; triethylamine / dichloromethane / 16 h / 20 °C / Cooling with ice View Scheme
参考文献
Ichikawa, Masanori; Yokomizo, Aki; Itoh, Masao; Haginoya, Noriyasu; Sugita, Kazuyuki; Usui, Hiroyuki; Terayama, Koji; Kanda, Akira
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 17 p. 5207 - 5224
75-84-3
新戊醇
→
反应条件
922162-82-1
反应条件
1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran; toluene / 2 h / 0 °C 2: hydrogen / ethyl acetate / 7 h / 20 °C 3: 4-(N,N-dimethlyamino)pyridine; triethylamine / dichloromethane / 16 h / 20 °C / Cooling with ice View Scheme
参考文献
Ichikawa, Masanori; Yokomizo, Aki; Itoh, Masao; Haginoya, Noriyasu; Sugita, Kazuyuki; Usui, Hiroyuki; Terayama, Koji; Kanda, Akira
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 17 p. 5207 - 5224
611-07-4
2-硝基-5-氯苯酚
→
反应条件
922162-82-1
反应条件
1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran; toluene / 2 h / 0 °C 2: hydrogen / ethyl acetate / 7 h / 20 °C 3: 4-(N,N-dimethlyamino)pyridine; triethylamine / dichloromethane / 16 h / 20 °C / Cooling with ice View Scheme
参考文献
Ichikawa, Masanori; Yokomizo, Aki; Itoh, Masao; Haginoya, Noriyasu; Sugita, Kazuyuki; Usui, Hiroyuki; Terayama, Koji; Kanda, Akira
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 17 p. 5207 - 5224
