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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
922162-88-7
合成路线
（共 4 条）
922162-87-6
→
反应条件
922162-88-7
反应条件
palladium 10 on activated carbon; hydrogen in water; ethyl acetate T=20°C; 7 h;
参考文献
Ichikawa, Masanori; Yokomizo, Aki; Itoh, Masao; Haginoya, Noriyasu; Sugita, Kazuyuki; Usui, Hiroyuki; Terayama, Koji; Kanda, Akira
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 17 p. 5207 - 5224
3282-30-2
三甲基乙酰氯
→
反应条件
922162-88-7
反应条件
1: sodium hydrogencarbonate / dichloromethane / 1.5 h / 0 - 20 °C 2: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran; toluene / 2 h / 0 °C 3: palladium 10 on activated carbon; hydrogen / water; ethyl acetate / 7 h / 20 °C View Scheme
参考文献
Ichikawa, Masanori; Yokomizo, Aki; Itoh, Masao; Haginoya, Noriyasu; Sugita, Kazuyuki; Usui, Hiroyuki; Terayama, Koji; Kanda, Akira
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 17 p. 5207 - 5224
28443-50-7
2-氨基-5-氯苯酚
→
反应条件
922162-88-7
反应条件
1: sodium hydrogencarbonate / dichloromethane / 1.5 h / 0 - 20 °C 2: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran; toluene / 2 h / 0 °C 3: palladium 10 on activated carbon; hydrogen / water; ethyl acetate / 7 h / 20 °C View Scheme
参考文献
Ichikawa, Masanori; Yokomizo, Aki; Itoh, Masao; Haginoya, Noriyasu; Sugita, Kazuyuki; Usui, Hiroyuki; Terayama, Koji; Kanda, Akira
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 17 p. 5207 - 5224
116278-66-1
→
反应条件
922162-88-7
反应条件
1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran; toluene / 2 h / 0 °C 2: palladium 10 on activated carbon; hydrogen / water; ethyl acetate / 7 h / 20 °C View Scheme
参考文献
Ichikawa, Masanori; Yokomizo, Aki; Itoh, Masao; Haginoya, Noriyasu; Sugita, Kazuyuki; Usui, Hiroyuki; Terayama, Koji; Kanda, Akira
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 17 p. 5207 - 5224
