10-(6-((2-氨基乙基)氨基)己基)-3,6-双(二甲基氨基)吖啶鎓氯化物四盐酸盐合成路线 (共 5 条)
反应条件
1: NaHCO3 / xylene / Heating
2: 0.1 M HCl / ethanol / Heating
3: 48percent HBr / 95 °C
4: 2.) HCl / 1.) CH3OH, reflux; 2.) C2H5OH
View Scheme
参考文献
Bowler; Ahmed; Sundquist; Hollis; Whang; Lippard
Journal of the American Chemical Society, 1989 , vol. 111, # 4 p. 1299 - 1306
反应条件
1: NaHCO3 / xylene / Heating
2: 0.1 M HCl / ethanol / Heating
3: 48percent HBr / 95 °C
4: 2.) HCl / 1.) CH3OH, reflux; 2.) C2H5OH
View Scheme
参考文献
Bowler; Ahmed; Sundquist; Hollis; Whang; Lippard
Journal of the American Chemical Society, 1989 , vol. 111, # 4 p. 1299 - 1306
反应条件
1: 0.1 M HCl / ethanol / Heating
2: 48percent HBr / 95 °C
3: 2.) HCl / 1.) CH3OH, reflux; 2.) C2H5OH
View Scheme
参考文献
Bowler; Ahmed; Sundquist; Hollis; Whang; Lippard
Journal of the American Chemical Society, 1989 , vol. 111, # 4 p. 1299 - 1306
反应条件
1: 48percent HBr / 95 °C
2: 2.) HCl / 1.) CH3OH, reflux; 2.) C2H5OH
View Scheme
参考文献
Bowler; Ahmed; Sundquist; Hollis; Whang; Lippard
Journal of the American Chemical Society, 1989 , vol. 111, # 4 p. 1299 - 1306
反应条件
hydrogenchloride
1.) CH3OH, reflux; 2.) C2H5OH; Multistep reaction;
参考文献
Bowler; Ahmed; Sundquist; Hollis; Whang; Lippard
Journal of the American Chemical Society, 1989 , vol. 111, # 4 p. 1299 - 1306